[R,(+)]-3,7-Dimethyl-7-octenal

Base Information

Chemical Name:[R,(+)]-3,7-Dimethyl-7-octenal
CAS No.:105485-65-2
Molecular Formula:C10H18O
Molecular Weight:154.252
Hs Code.:
Mol file:105485-65-2.mol

Synonyms:[R,(+)]-3,7-Dimethyl-7-octenal

Suppliers and Price of [R,(+)]-3,7-Dimethyl-7-octenal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of [R,(+)]-3,7-Dimethyl-7-octenal

Chemical Property:

Boiling Point:51 °C (1.4 mmHg)
PSA：17.07000
LogP:2.95790

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [R,(+)]-3,7-Dimethyl-7-octenal

There total 1 articles about [R,(+)]-3,7-Dimethyl-7-octenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141-26-4,86951-91-9,105485-65-2
(R)-3,7-dimethyl-oct-7-enal

Guidance literature:: With aluminum oxide; at 350 ℃;
DOI:10.1021/jo01067a007

Reference yield:

: 105485-65-2
rhodinal

: 75983-36-7,85785-47-3,85785-48-4,85880-35-9,85880-36-0,85880-37-1,85880-38-2
4(RS),8(S)-dimethyldecanal

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 2 h / Heating

2: 1) NaBH₄, BF₃*Et₂O, 2) 30percent H₂O₂, 3N aq. NaOH / 1) THF, 12 h, 2) 25 deg C, 8 h

3: 80 percent / PPh₃, Br₂ / CH₂Cl₂; CCl₄ / Ambient temperature

4: 1) NaH / 1) benzene, DMF, 2 h, 2) 100 deg C, 4 h

5: 98 percent / KOAc, H₂O / dimethylsulfoxide / 6 h / Heating

6: 88 percent / LAH / diethyl ether

7: 88 percent / PCC / CH₂Cl₂ / 1 h

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; water; dihydrogen peroxide; bromine; potassium acetate; sodium hydride; hydrazine hydrate; triphenylphosphine; pyridinium chlorochromate; In tetrachloromethane; diethyl ether; dichloromethane; dimethyl sulfoxide; diethylene glycol;

Reference yield:

: 141-26-4,86951-91-9,105485-65-2
(R)-3,7-dimethyl-oct-7-enal

: 925-69-9,1730-98-9
(S)-6-methyl-octan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O, KOH / bis-(2-hydroxy-ethyl) ether

2: O₃, O₂, Zn, aq. AcOH

With potassium hydroxide; oxygen; ozone; hydrazine hydrate; acetic acid; zinc; In diethylene glycol;
DOI:10.1021/jo01067a007