bis(2-bicyclo[2.2.1]heptanyl)phosphane;chloropalladium(1+);N,N-dimethyl-2-phenylaniline

Base Information

• Chemical Name: bis(2-bicyclo[2.2.1]heptanyl)phosphane;chloropalladium(1+);N,N-dimethyl-2-phenylaniline
• CAS No.: 359803-53-5
• Molecular Formula: C₂₈H₃₇ClNPPd
• Molecular Weight: 560.455
• Hs Code.: 28439000
• European Community (EC) Number: 811-496-0
• Mol file: 359803-53-5.mol

Synonyms:359803-53-5;SCHEMBL734873;2,-(DImethylamino)-2-biphenylyl-palladium(II) chloride Dinorbornylphosphine

Chemical Property of bis(2-bicyclo[2.2.1]heptanyl)phosphane;chloropalladium(1+);N,N-dimethyl-2-phenylaniline

Chemical Property:

• Melting Point: 160-170 °C (dec.)(lit.)
• PSA: 16.83000
• LogP: 7.95140
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 559.13870
• Heavy Atom Count: 32
• Complexity: 543

Purity/Quality:

98% ^*data from raw suppliers

CHLORO(DI-2-NORBORNYLPHOSPHINO)(2'-DIMETHYLAMINO-1,1'-BIPHENYL-2-YL)PALLADIUM (II) 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=CC=C1C2=CC=CC=[C-]2.C1CC2CC1CC2PC3CC4CCC3C4.Cl[Pd+]

Technology Process of bis(2-bicyclo[2.2.1]heptanyl)phosphane;chloropalladium(1+);N,N-dimethyl-2-phenylaniline

There total 1 articles about bis(2-bicyclo[2.2.1]heptanyl)phosphane;chloropalladium(1+);N,N-dimethyl-2-phenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

HP(2-norbornyl)2 (148432-44-4) + bis(N,N-dimethyl-2-aminobiphenyl)dipalladium-μ-dichloride (119326-02-2) → 2'-(dimethylamino)-2-biphenylyl-palladium(II) chloride dinorbornylphosphine complex (359803-53-5)

Guidance literature:

In dichloromethane; (Ar), Pd complex as suspn. in CH2Cl2 treated with phosphane; filtered, (plug of silica), concd., pptd.(hexane);

DOI:10.1002/1521-3773(20021004)41:19<3668::AID-ANIE3668>3.0.CO;2-U

upstream raw materials:

HP(2-norbornyl)2

bis(N,N-dimethyl-2-aminobiphenyl)dipalladium-μ-dichloride

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