2,3,4-Tri-O-acetyl-beta-D-xylopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3,4-Tri-O-acetyl-beta-D-xylopyranosyl trichloroacetimidate
CAS No.:128377-34-4
Molecular Formula:C₁₃H₁₆Cl₃NO₈
Molecular Weight:420.631
Hs Code.:2938909090
Mol file:128377-34-4.mol

Synonyms:2,3,4,4'-TETRACB UNLABELED;

Suppliers and Price of 2,3,4-Tri-O-acetyl-beta-D-xylopyranosyl trichloroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSYL TRICHLOROACETIMIDATE 95.00%
5MG
$ 501.08

Total 5 raw suppliers

Chemical Property of 2,3,4-Tri-O-acetyl-beta-D-xylopyranosyl trichloroacetimidate

Chemical Property:

Boiling Point:395.3±52.0 °C(Predicted)
PKA:1.39±0.70(Predicted)
PSA：121.21000
Density:1.58±0.1 g/cm3(Predicted)
LogP:1.60160

Purity/Quality:

99% ^*data from raw suppliers

2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSYL TRICHLOROACETIMIDATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3,4-Tri-O-acetyl-beta-D-xylopyranosyl trichloroacetimidate

There total 2 articles about 2,3,4-Tri-O-acetyl-beta-D-xylopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106820-14-8
2,3,4-Tri-O-acetyl-D-xylopyranose

: 545-06-2
trichloroacetonitrile

: 128377-34-4,869848-87-3
2,3,4-tri-O-acetyl-β-D-xylopyranoside trichloroacetimidate

: 128376-91-0,869848-87-3
2,3,4-tri-O-acetyl-α-D-xylopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at -20 ℃; for 4h;
DOI:10.1016/0008-6215(90)84167-S

Reference yield:

: 62446-93-9
1,2,3,4-tetra-O-acetyl-D-xylopyranose

: 128377-34-4,869848-87-3
2,3,4-tri-O-acetyl-β-D-xylopyranoside trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NH₂NH₂*AcOH / dimethylformamide / 0.25 h / 55 °C

2: 16 percent / DBU / CH₂Cl₂ / 4 h / -20 °C

With hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84167-S

Reference yield:

: 1338564-86-5
C₁₈H₂₂O₁₀

: 128377-34-4,869848-87-3
2,3,4-tri-O-acetyl-β-D-xylopyranoside trichloroacetimidate

: C₂₉H₃₆O₁₇

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere; Molecular sieve;
DOI:10.1080/10286020.2011.596830