1-(8-Acetyl-quinolin-2-yl)-ethanone

Base Information

• Chemical Name: 1-(8-Acetyl-quinolin-2-yl)-ethanone
• CAS No.: 1214264-82-0
• Molecular Formula: C13H11NO2
• Molecular Weight: 213.23194
• Mol file: 1214264-82-0.mol

Synonyms:1-(8-Acetyl-quinolin-2-yl)-ethanone

Chemical Property of 1-(8-Acetyl-quinolin-2-yl)-ethanone

Chemical Property:

• PSA: 47.03000
• LogP: 2.64000

Purity/Quality:

97% ^*data from raw suppliers

2,8-Diacetylquinoline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(8-Acetyl-quinolin-2-yl)-ethanone

There total 1 articles about 1-(8-Acetyl-quinolin-2-yl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.5%

diethyl quinoline-2,8-dicarboxylate (1214264-83-1) → 2,8-diacetyl-quinoline (1214264-82-0)

Guidance literature:

diethyl quinoline-2,8-dicarboxylate; With sodium ethanolate; In ethyl acetate; for 9h; Reflux;

With hydrogenchloride; for 6h; Reflux;

DOI:10.1021/om9010142

Reference yield: 78.0%

2,8-diacetyl-quinoline (1214264-82-0) + 2,6-dimethylaniline (87-62-7) → 2,8-bis[1-(2,6-dimethylphenylimino)ethyl]quinoline (1214264-74-0)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 24h; Reflux;

DOI:10.1021/om9010142

Reference yield: 67.0%

2,6-diethylaniline (579-66-8) + 2,8-diacetyl-quinoline (1214264-82-0) → 2,8-bis[1-(2,6-diethylphenylimino)ethyl]quinoline (1214264-75-1)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 24h; Reflux;

DOI:10.1021/om9010142

upstream raw materials:

diethyl quinoline-2,8-dicarboxylate

Downstream raw materials:

2,8-bis[1-(2,6-diethylphenylimino)ethyl]quinoline

2,8-bis[1-(2,6-dimethylphenylimino)ethyl]quinoline

2,8-bis[1-(2,4,6-trimethylphenylimino)ethyl]quinoline

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