1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

Base Information

Chemical Name:1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine
CAS No.:503149-20-0
Molecular Formula:C₂₀H₂₁N₅O₂
Molecular Weight:363.419
Hs Code.:
Mol file:503149-20-0.mol

Synonyms:1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

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Chemical Property of 1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

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Technology Process of 1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

There total 3 articles about 1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10315-00-1
1-benzyloxycarbonylisonipecotic acid anilide

: 503149-20-0
1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

Guidance literature:: With trimethylsilylazide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 20 ℃; for 120h; Cooling with ice;
DOI:10.1016/j.bmc.2012.08.012

Reference yield:

: 4648-54-8
trimethylsilylazide

: 10315-00-1
1-benzyloxycarbonylisonipecotic acid anilide

: 503149-20-0
1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 0 - 20 ℃; for 120h;

Reference yield:

: 10314-98-4
1-benzyloxycarbonylpiperidine-4-carboxylic acid

: 503149-20-0
1-benzyloxycarbonyl-4-(1-phenyl-1H-tetrazol-5-yl)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: aniline; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran / 17 h / 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate; trimethylsilylazide / tetrahydrofuran; toluene / 120 h / 20 °C / Cooling with ice

With trimethylsilylazide; di-isopropyl azodicarboxylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; aniline; triphenylphosphine; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmc.2012.08.012