Fmoc-L-Thr(β-D-Lac(Ac)7)-OH

Base Information

• Chemical Name: Fmoc-L-Thr(β-D-Lac(Ac)7)-OH
• CAS No.: 657395-98-7
• Molecular Formula: C45H53NO22
• Molecular Weight: 959.9
• Mol file: 657395-98-7.mol

Synonyms:Fmoc-L-Thr(β-D-Lac(Ac)7)-OH;N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-[2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-beta-D-galactopyranosyl)-beta-D-glucopyranosyl]-L-threonine

Chemical Property of Fmoc-L-Thr(β-D-Lac(Ac)7)-OH

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Fmoc-Thr(beta-D-Lac(Ac)7)-OH ^*data from reagent suppliers

Safty Information:

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Technology Process of Fmoc-L-Thr(β-D-Lac(Ac)7)-OH

There total 11 articles about Fmoc-L-Thr(β-D-Lac(Ac)7)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

Nα-fluoren-9-ylmethoxycarbonyl-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-L-threonine benzyl ester → Nα-fluoren-9-ylmethoxycarbonyl-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-L-threonine (657395-98-7)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; under 760.051 Torr;

DOI:10.1002/psc.2826

Reference yield: 65.0%

Nα-fluoren-9-ylmethoxycarbonyl-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-L-threonine benzyl ester → Nα-fluoren-9-ylmethoxycarbonyl-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-L-threonine (657395-98-7)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In methanol; under 760.051 Torr;

DOI:10.1002/psc.2826

Reference yield: 60.0%

Nα-fluoren-9-ylmethoxycarbonyl-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-L-threonine benzyl ester → Nα-fluoren-9-ylmethoxycarbonyl-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-L-threonine (657395-98-7)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; under 760.051 Torr;

DOI:10.1002/psc.2826

upstream raw materials:

Fmoc-Thr-OH

β-cellobioseoctaacetate

1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose

N-(fluoren-9-ylmethoxycarbonyl)-L-threonine benzyl ester

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