Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]-

Base Information

• Chemical Name: Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]-
• CAS No.: 1533-78-4
• Deprecated CAS: 79300-13-3,375793-86-5,375793-86-5
• Molecular Formula: C22H24 Cl N5 O7
• Molecular Weight: 505.915
• European Community (EC) Number: 216-251-6
• UNII: 659W3QZ0KS
• DSSTox Substance ID: DTXSID3061764
• Nikkaji Number: J38.443G
• Wikidata: Q27263859
• Mol file: 1533-78-4.mol

Synonyms:1533-78-4;Disperse Red 354;CCRIS 8991;Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]-;EINECS 216-251-6;UNII-659W3QZ0KS;2-[3-acetamido-N-(2-acetyloxyethyl)-4-[(2-chloro-4-nitrophenyl)diazenyl]anilino]ethyl acetate;659W3QZ0KS;79300-13-3;3-((N,N-Diacetyloxyethyl)amino)-6-((2'-chloro-4'-nitrophenyl)azo)acetanilide;Acetamide, N-(5-(bis(2-(acetyloxy)ethyl)amino)-2-((2-chloro-4-nitrophenyl)azo)phenyl)-;2,2'-((3-Acetamido-4-((2-chloro-4-nitrophenyl)azo)phenyl)imino)diethyl diacetate;5'-(Bis(2-hydroxyethyl)amino)-2'-((2-chloro-4-nitrophenyl)azo)acetanilide, diacetate (ester);Acetamide, N-(5-(bis(2-(acetyloxy)ethyl)amino)-2-(2-(2-chloro-4-nitrophenyl)diazenyl)phenyl)-;2,2'-[[3-Acetamido-4-[(2-chloro-4-nitrophenyl)azo]phenyl]Imino]diethyl diacetate;Acetamide,N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]-;Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[2-(2-chloro-4-nitrophenyl)diazenyl]phenyl]-;C.I.Disperse Red 354;DIANIX RUBINE S 2G;C.I. Disperse Red 354;CI DISPERSE RED 354;DTXSID3061764;SCHEMBL12955792;SCHEMBL21127849;CI DISPERSE RED 167:1;LS-164901;CI 11338:1;W-109677;Q27263859;Acetamide, N-[5-[bis[2-(acetyloxy)ethyl] amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl] -;BIS(2-ACETOXYETHYL)AMINO-2'-(2-CHLORO-4-NITROPHENYLAZO)ACETANILIDE, 5'-;ACETANILIDE, 5'-(BIS(2-HYDROXYETHYL)AMINO)-2'-((2-CHLORO-4-NITROPHENYL)AZO)-, DIACETATE;ACETANILIDE, 5'-(BIS(2-HYDROXYETHYL)AMINO)-2'-((2-CHLORO-4-NITROPHENYL)AZO)-, DIACETATE (ESTER)

Chemical Property of Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]-

Chemical Property:

• Vapor Pressure: 7.59E-20mmHg at 25°C
• Melting Point: 127 ºC
• Refractive Index: 1.6
• Boiling Point: 707.2°Cat760mmHg
• PKA: 14.17±0.70(Predicted)
• Flash Point: 381.5°C
• PSA: 155.48000
• Density: 1.36
• LogP: 5.15080
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 12
• Exact Mass: 505.1364258
• Heavy Atom Count: 35
• Complexity: 758

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=C(C=CC(=C1)N(CCOC(=O)C)CCOC(=O)C)N=NC2=C(C=C(C=C2)[N+](=O)[O-])Cl

Technology Process of Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]-

There total 6 articles about Acetamide, N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(N,N-di(acetyloxyethyl)amino)-N-phenylacetamide (27059-08-1) + 2-Chloro-4-nitroaniline (121-87-9) → N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]acetamide (1533-78-4,79300-13-3)

Guidance literature:

With 1-ethenyl-2-pyrrolidinone; nitrosylsulfuric acid; sulfuric acid; ammonia; urea; In water; at 5 - 65 ℃; for 1h; pH=5 - 6; Concentration; pH-value; Temperature; Large scale;

Reference yield:

C6H3ClN3O2(1+)*HO4S(1-) + 3-(N,N-di(acetyloxyethyl)amino)-N-phenylacetamide (27059-08-1) → N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]acetamide (1533-78-4,79300-13-3)

Guidance literature:

With peregal; In water; at 20 - 75 ℃; for 6h; Temperature;

Reference yield:

N,N-diacetoxyethyl-m-aminoacetanilide + 2-Chloro-4-nitroaniline (121-87-9) → N-[5-[bis[2-(acetyloxy)ethyl]amino]-2-[(2-chloro-4-nitrophenyl)azo]phenyl]acetamide (1533-78-4,79300-13-3)

Guidance literature:

2-Chloro-4-nitroaniline; With nitrosylsulfuric acid; sulfuric acid; In water;

N,N-diacetoxyethyl-m-aminoacetanilide; With aminosulfonic acid; In water; at 15 - 35 ℃; for 1h; Reagent/catalyst; Temperature;

upstream raw materials:

3-(N,N-di(acetyloxyethyl)amino)-N-phenylacetamide

2-Chloro-4-nitroaniline

2C₆H₃ClN₃O₂⁽¹⁺⁾*O₄S^(2-)