4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide

Base Information

Chemical Name:4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide
CAS No.:317337-07-8
Molecular Formula:C9H9N5OS2
Molecular Weight:267.335
Hs Code.:
Mol file:317337-07-8.mol

Synonyms:4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide;N-(4-(5-Mercapto-1,3,4-oxadiazol-2-yl)phenyl)hydrazinecarbothioaMide

Suppliers and Price of 4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-(4-(5-Mercapto-1,3,4-oxadiazol-2-yl)phenyl)hydrazinecarbothioamide 95+%
1g
$ 496.00

Total 5 raw suppliers

Chemical Property of 4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide

Chemical Property:

PSA：159.89000
LogP:2.34960

Purity/Quality:

97% ^*data from raw suppliers

N-(4-(5-Mercapto-1,3,4-oxadiazol-2-yl)phenyl)hydrazinecarbothioamide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide

There total 4 articles about 4-(4-(5-Mercapto-1,3,4- oxadiazol-2-yl)phenyl) thioseMicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5-(4-isothiocyanatophenyl)-1,3,4-oxadiazole-2-thiol

: 317337-07-8
hydrazino-4-(5-sulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: With hydrazine; In benzene; for 3h; Reflux;
DOI:10.1016/j.bmc.2011.09.038

Reference yield:

: 203268-83-1,32058-82-5
5-(4-aminophenyl)-1,3,4-oxadiazole-2-thiol

: 317337-07-8
hydrazino-4-(5-sulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

2: hydrazine hydrate / toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; In acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 5351-17-7
4-aminobenzohydrazide

: 317337-07-8
hydrazino-4-(5-sulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

1.2: pH 4

2.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

3.1: hydrazine hydrate / toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017