(E)-3-Methyl-2-undecene

Base Information

Chemical Name:(E)-3-Methyl-2-undecene
CAS No.:74630-47-0
Molecular Formula:C₁₂H₂₄
Molecular Weight:168.323
Hs Code.:
Mol file:74630-47-0.mol

Synonyms:(E)-3-Methyl-2-undecene

Suppliers and Price of (E)-3-Methyl-2-undecene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of (E)-3-Methyl-2-undecene

Chemical Property:

PSA：0.00000
LogP:4.70320

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-3-Methyl-2-undecene

There total 17 articles about (E)-3-Methyl-2-undecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 30089-00-0
9-octyl-9-bora-bicyclo[3.3.1]nonane

: 3017-69-4
2-methyl-1-propenylbromide

: 57024-90-5,74630-47-0
(Z)-3-Methyl-2-undecene

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; cis-dichloro-1,1'-bis(diphenylphosphino)ferrocene palladium(II); In tetrahydrofuran; To a soln. of 9-octyl-9-BBN is added (CH3)2CCHBr, THF and aq. NaOH at room temp., mixt. refluxed overnight (14-16 h), react. mixt. diluted with hexane or benzene, residue oxidized by H2O2 at room temp.; Extracted, washed with brine, dried (MgSO4), final product is identified by mass spectrometry, IR, elem. anal.;
DOI:10.1021/ja00183a048

Reference yield: 91.0%

: 3017-68-3
(Z)-2-Bromo-2-butene

: 111-66-0,25068-25-1
oct-1-ene

: 57024-90-5,74630-47-0
(Z)-3-Methyl-2-undecene

Guidance literature:: oct-1-ene; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 ℃; for 2h;

(Z)-2-Bromo-2-butene; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide; In tetrahydrofuran; water; for 14h; Reflux;
DOI:10.1021/acs.joc.6b02917

Reference yield: 84.0%

: 3017-71-8
(E)-2-bromobut-2-ene

: 38841-98-4
n-octylmagnesium chloride

: 74630-47-0
(E)-3-methylundec-2-ene

Guidance literature:: With 1-methyl-pyrrolidin-2-one; iron(III)-acetylacetonate; In tetrahydrofuran; at -5 - 0 ℃; for 0.25h;
DOI:10.1055/s-1998-2135