erythro-Guaiacylglycerol β-sinapyl ether

Base Information

Chemical Name:erythro-Guaiacylglycerol β-sinapyl ether
CAS No.:877875-96-2
Molecular Formula:C₂₁H₂₆O₈
Molecular Weight:406.433
Hs Code.:
Mol file:877875-96-2.mol

Synonyms:erythro-Guaiacylglycerol β-sinapyl ether;(1S,2R)-1-(4-Hydroxy-3-methoxyphenyl)-2-[4-[(1E)-3-hydroxy-1-propenyl]-2,6-dimethoxyphenoxy]-1,3-propanediol;erythro-Guaiacylglycerol beta-sinapyl ether

Suppliers and Price of erythro-Guaiacylglycerol β-sinapyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
erythro-Guaiacylglycerolβ-sinapylether 95+%
5mg
$ 922.00

Total 6 raw suppliers

Chemical Property of erythro-Guaiacylglycerol β-sinapyl ether

Chemical Property:

PSA：117.84000
LogP:1.89680

Purity/Quality:

98.0% ^*data from raw suppliers

erythro-Guaiacylglycerolβ-sinapylether 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of erythro-Guaiacylglycerol β-sinapyl ether

There total 13 articles about erythro-Guaiacylglycerol β-sinapyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₅₈O₈Si₂

: 887914-26-3,877875-96-2
(1R,2S)-1-(4-hydroxy-3-methoxyphenyl)-2-(4-((E)-3-hydroxyprop-1-en-1-yl)-2,6-dimethoxyphenoxy)propane-1,3-diol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1039/c6ra22026f

Reference yield:

: 1186295-11-3
(7S,8R)-guaiacylglycerol-8-O-4'-sinapyl ether 9'-O-β-D-glucopyranoside

: 877875-96-2
(1S,2R)-1-(4-hydroxy-3-methoxyphenyl)-2-({4-[(E)-3-hydroxyprop-1-enyl]-2,6-dimethoxyphenyl}oxy)propane-1,3-diol

Guidance literature:: With water; cellulase; at 40 ℃; for 96h; Enzymatic reaction;
DOI:10.3390/molecules14030953

Reference yield:

: 106852-80-6
4-(t-butyldimethylsilyloxy)-3,5-dimethoxybenzaldehyde

: 887914-26-3,877875-96-2
(1R,2S)-1-(4-hydroxy-3-methoxyphenyl)-2-(4-((E)-3-hydroxyprop-1-en-1-yl)-2,6-dimethoxyphenoxy)propane-1,3-diol

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / neat (no solvent) / 4 h / 20 °C

1.2: 3 h / 20 °C

2.1: lithium aluminium tetrahydride; benzyl chloride / tetrahydrofuran / 0 - 20 °C

3.1: potassium carbonate; potassium iodide / acetone / 0.25 h / 20 °C

3.2: 20 °C

4.1: 1H-imidazole / dichloromethane / 0.5 h / 0 °C

4.2: 2 h / 0 - 20 °C

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

5.2: 1 h / Inert atmosphere

6.1: sodium tetrahydroborate / tetrahydrofuran; water / 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; potassium carbonate; benzyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1039/c6ra22026f