Technology Process of 2-Hydroxy-4-methoxy-3,5,6-trimethylbenzoic acid
There total 9 articles about 2-Hydroxy-4-methoxy-3,5,6-trimethylbenzoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; water;
In
dimethyl sulfoxide;
at 90 - 95 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / glacial acetic acid, H2 / 10percent Pd/C / ethyl acetate / 70 h / 45 °C
2: 92 percent / potassium carbonate / acetone / 22 h / Heating
3: 53 percent / potassium hydroxide, H2O / dimethylsulfoxide / 4 h / 90 - 95 °C
With
potassium hydroxide; water; hydrogen; potassium carbonate; acetic acid;
palladium on activated charcoal;
In
dimethyl sulfoxide; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 92 percent / potassium carbonate / acetone / 22 h / Heating
2: 53 percent / potassium hydroxide, H2O / dimethylsulfoxide / 4 h / 90 - 95 °C
With
potassium hydroxide; water; potassium carbonate;
In
dimethyl sulfoxide; acetone;
