1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

Base Information

Chemical Name:1-(4,5-dimethoxy-2-nitrophenyl)diazoethane
CAS No.:154140-56-4
Molecular Formula:C₁₀H₁₁N₃O₄
Molecular Weight:237.215
Hs Code.:
Mol file:154140-56-4.mol

Synonyms:1-(4,5-dimethoxy-2-nitrophenyl)diazoethane;1-(2-Diazoethyl)-4,5-diMethoxy-2-nitrobenzene

Suppliers and Price of 1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

There total 4 articles about 1-(4,5-dimethoxy-2-nitrophenyl)diazoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123642-61-5
4,5-dimethoxy-2-nitroacetophenone hydrazone

: 116271-29-5,154140-56-4
1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

Guidance literature:: With manganese(IV) oxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1002/anie.200503339

Reference yield:

: [1-(4,5-Dimethoxy-2-nitro-phenyl)-eth-(E)-ylidene]-hydrazine

: 116271-29-5,154140-56-4
1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

Guidance literature:: With manganese(IV) oxide; In chloroform; for 0.0833333h; Ambient temperature;
DOI:10.1246/bcsj.71.1923

Reference yield:

: 4101-32-0
4',5'-dimethoxy-2'-nitroacetophenone

: 116271-29-5,154140-56-4
1-(4,5-dimethoxy-2-nitrophenyl)diazoethane

Guidance literature:: Multi-step reaction with 2 steps

1: hyrazine monohydrate, acetic acid / ethanol / 3 h / Heating

2: MnO₂ / CHCl₃ / 0.08 h / Ambient temperature

With manganese(IV) oxide; hydrazine hydrate; acetic acid; In ethanol; chloroform;
DOI:10.1246/bcsj.71.1923