Technology Process of 7-Oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt
There total 5 articles about 7-Oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid sodium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
tetrahydrofuran;
for 0.0833333h;
DOI:10.1039/P19810003242
- Guidance literature:
-
Multi-step reaction with 5 steps
1: benzene / Heating
2: 1.) 2,6-lutidine, 2.) thionyl chloride / 1) THF
3: 2,6-lutidine / dioxane / Ambient temperature
4: 1.) ozone, trifluoroacetic acid, 2.) triphenylphosphine, 3.) aq. sodium hydrogencarbonate / 1) ethyl acetate
5: aq. sodium hydroxide / tetrahydrofuran / 0.08 h
With
2,6-dimethylpyridine; sodium hydroxide; thionyl chloride; sodium hydrogencarbonate; ozone; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; benzene;
DOI:10.1039/P19810003242
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) 2,6-lutidine, 2.) thionyl chloride / 1) THF
2: 2,6-lutidine / dioxane / Ambient temperature
3: 1.) ozone, trifluoroacetic acid, 2.) triphenylphosphine, 3.) aq. sodium hydrogencarbonate / 1) ethyl acetate
4: aq. sodium hydroxide / tetrahydrofuran / 0.08 h
With
2,6-dimethylpyridine; sodium hydroxide; thionyl chloride; sodium hydrogencarbonate; ozone; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/P19810003242
