1-BroMo-5-isopropoxy-2-Methyl-4-nitrobenzene

Base Information

• Chemical Name: 1-BroMo-5-isopropoxy-2-Methyl-4-nitrobenzene
• CAS No.: 1202858-68-1
• Molecular Formula: C10H12BrNO3
• Molecular Weight: 274.11118
• Mol file: 1202858-68-1.mol

Synonyms:1-BroMo-5-isopropoxy-2-Methyl-4-nitrobenzene;2-BroMo-4-isopropoxy-5-nitrotoluene

Chemical Property of 1-BroMo-5-isopropoxy-2-Methyl-4-nitrobenzene

Chemical Property:

• Boiling Point: 342.1±37.0 °C(Predicted)
• PSA: 55.05000
• Density: 1.434±0.06 g/cm3(Predicted)
• LogP: 3.97610
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

2-Bromo-4-isopropoxy-5-nitrotoluene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-BroMo-5-isopropoxy-2-Methyl-4-nitrobenzene

There total 4 articles about 1-BroMo-5-isopropoxy-2-Methyl-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.7%

1-bromo-5-fluoro-2-methyl-4-nitrobenzene (64695-96-1) + isopropyl alcohol (67-63-0,8013-70-5) → 1-bromo-5-isopropoxy-2-methyl-4-nitrobenzene (1202858-68-1)

Guidance literature:

With caesium carbonate; at 60 ℃; for 16h; Inert atmosphere;

Reference yield:

2-bromo-4-isopropoxy-1-methylbenzene (1254062-68-4) → 1-bromo-5-isopropoxy-2-methyl-4-nitrobenzene (1202858-68-1)

Guidance literature:

With nitric acid; at 20 ℃; for 2h;

Reference yield:

2-bromo-4-fluorotoluene (1422-53-3) → 1-bromo-5-isopropoxy-2-methyl-4-nitrobenzene (1202858-68-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid; potassium nitrite / water / 15.75 h / 0 - 25 °C

2: caesium carbonate / 15 h / Reflux

With potassium nitrite; sulfuric acid; caesium carbonate; In water;

upstream raw materials:

1-bromo-5-fluoro-2-methyl-4-nitrobenzene

isopropyl alcohol

2-bromo-4-fluorotoluene

3-bromo-p-cresol

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