CID 11184067

Base Information

• Chemical Name: CID 11184067
• CAS No.: 16595-76-9
• Molecular Formula: C11H12 N2 S . Cl H
• Molecular Weight: 240.757
• Hs Code.: 2934100090
• Mol file: 16595-76-9.mol

Synonyms:

Chemical Property of CID 11184067

Chemical Property:

• Vapor Pressure: 6.61E-05mmHg at 25°C
• Boiling Point: 344.4°C at 760 mmHg
• Flash Point: 162.1°C
• PSA: 40.90000
• LogP: 2.32160
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 240.0487973
• Heavy Atom Count: 15
• Complexity: 256

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CSC2=[N+]1CC(N2)C3=CC=CC=C3.[Cl-]
• Isomeric SMILES: C1CSC2=[N+]1C[C@H](N2)C3=CC=CC=C3.[Cl-]

Technology Process of CID 11184067

There total 1 articles about CID 11184067 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tetramisole (5036-02-2) → levamisole hydrochloride (16595-80-5,74191-78-9) + (+)-Tetramisole hydrochloride (16595-76-9,74191-78-9)

Guidance literature:

With hydrogenchloride; In isopropyl alcohol; toluene; Title compound not separated from byproducts;

DOI:10.1016/S0040-4020(01)96641-4

Reference yield:

levamisole hydrochloride (4641-34-3,5086-74-8,16595-76-9,16595-80-5,24240-85-5,24593-45-1,74191-78-9) → C22H24N6O4S2 (108291-54-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium nitrite, aq. HCl / H₂O / Ambient temperature

2: CHCl₃ / 48 h

With hydrogenchloride; sodium nitrite; In chloroform; water;

Reference yield:

levamisole hydrochloride (4641-34-3,5086-74-8,16595-76-9,16595-80-5,24240-85-5,24593-45-1,74191-78-9) → 1-(2-Mercapto-ethyl)-4-phenyl-imidazolidin-2-one (32190-33-3,69158-71-0,72105-94-3)

Guidance literature:

In water; at 99.9 ℃; for 576h;

upstream raw materials:

Tetramisole

Downstream raw materials:

1-(2-Mercapto-ethyl)-4-phenyl-imidazolidin-2-one

(E)-1-nitroso-2-oxo-3-(2-nitrosothioethyl)-5-phenylimidazolidine

C₂₂H₂₄N₆O₄S₂