2-Chloro-4-Methylcyclohex-1-en-1-carbaldehyd

Base Information

• Chemical Name: 2-Chloro-4-Methylcyclohex-1-en-1-carbaldehyd
• CAS No.: 38127-46-7
• Molecular Formula: C₈H₁₁ClO
• Molecular Weight: 158.628
• Mol file: 38127-46-7.mol

Synonyms:2-Chloro-4-Methylcyclohex-1-en-1-carbaldehyd;2-Chloro-4-methylcyclohex-1-ene-1-carboxaldehyde

Chemical Property of 2-Chloro-4-Methylcyclohex-1-en-1-carbaldehyd

Chemical Property:

• Boiling Point: 90-91℃ (9 Torr)
• PSA: 17.07000
• LogP: 2.49820

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Chloro-4-Methylcyclohex-1-en-1-carbaldehyd

There total 2 articles about 2-Chloro-4-Methylcyclohex-1-en-1-carbaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 3-Methylcyclohexanone (591-24-2,625-96-7) → 2-Chloro-4-methylcyclohex-1-en-1-carbaldehyd (38127-46-7) + 1-chloro-2-formyl-3-methylcyclohexene (85355-90-4)

Guidance literature:

With trichlorophosphate; In Trichloroethylene; at 55 - 60 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jo00159a032

Reference yield:

→ 2-Chloro-4-methylcyclohex-1-en-1-carbaldehyd (38127-46-7)

Guidance literature:

entspr. Cyclohexanon, Formylieren;

upstream raw materials:

N,N-dimethyl-formamide

3-Methylcyclohexanone

Refernces