1,3-Dioxolan-2-one, 5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1H-1,2,4-triazol-1-ylmethyl)-, (4R,5R)-

Base Information

Chemical Name:1,3-Dioxolan-2-one, 5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1H-1,2,4-triazol-1-ylmethyl)-, (4R,5R)-
CAS No.:96223-46-0
Molecular Formula:C₁₈H₁₂Cl₃N₃O₃
Molecular Weight:424.671
Hs Code.:

Synonyms:(4R,5R)-5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1,2,4-triazol-1-ylmethyl)-1,3-dioxolan-2-one;

Suppliers and Price of 1,3-Dioxolan-2-one, 5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1H-1,2,4-triazol-1-ylmethyl)-, (4R,5R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dioxolan-2-one, 5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1H-1,2,4-triazol-1-ylmethyl)-, (4R,5R)-

Chemical Property:

Boiling Point:629.7°Cat760mmHg
Flash Point:334.6°C
Density:1.56g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-Dioxolan-2-one, 5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1H-1,2,4-triazol-1-ylmethyl)-, (4R,5R)-

There total 10 articles about 1,3-Dioxolan-2-one, 5-(4-chlorophenyl)-4-(2,4-dichlorophenyl)-4-(1H-1,2,4-triazol-1-ylmethyl)-, (4R,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 93363-60-1,96223-50-6,96223-54-0,107538-66-9,107741-29-7,107741-30-0
(erythro)-1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-3-(1H-1,2,4-triazol-1-yl)propylene glycol

: 530-62-1
1,1'-carbonyldiimidazole

: 96223-41-5,96223-46-0,107659-67-6,107659-68-7
4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)-2-oxo-4-<(1H-1,2,4-triazol-1-yl)methyl>-1,3-dioxolane

Guidance literature:: In chloroform; for 1h; Heating;
DOI:10.1021/jm00389a016

Reference yield: 47.0%

: 93363-60-1,96223-50-6,96223-54-0,107538-66-9,107741-29-7,107741-30-0
(threo)-1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-3-(1H-1,2,4-triazol-1-yl)propylene glycol

: 530-62-1
1,1'-carbonyldiimidazole

: 96223-41-5,96223-46-0,107659-67-6,107659-68-7
4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)-2-oxo-4-<(1H-1,2,4-triazol-1-yl)methyl>1,3-dioxolane

Guidance literature:: In dichloromethane; for 1h; Heating;
DOI:10.1021/jm00389a016

Reference yield:

: 111299-34-4
(4-Chloro-phenyl)-[2-(2,4-dichloro-phenyl)-oxiranyl]-methanone

: 96223-41-5,96223-46-0,107659-67-6,107659-68-7
4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)-2-oxo-4-<(1H-1,2,4-triazol-1-yl)methyl>1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 17 h / 50 °C

2: 3 percent / NaBH₄ / ethanol / 1 h / Ambient temperature

3: 47 percent / CH₂Cl₂ / 1 h / Heating

With sodium tetrahydroborate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00389a016