3-METHYL-5-OXO-5-(3,4,5-TRIMETHOXYPHENYL)VALERIC ACID

Base Information

• Chemical Name: 3-METHYL-5-OXO-5-(3,4,5-TRIMETHOXYPHENYL)VALERIC ACID
• CAS No.: 101499-91-6
• Molecular Formula: C₁₅H₂₀O₆
• Molecular Weight: 296.32
• Hs Code.: 2918990090
• Mol file: 101499-91-6.mol

Synonyms:3-METHYL-5-OXO-5-(3,4,5-TRIMETHOXYPHENYL)VALERIC ACID

Chemical Property of 3-METHYL-5-OXO-5-(3,4,5-TRIMETHOXYPHENYL)VALERIC ACID

Chemical Property:

• Vapor Pressure: 1.05E-09mmHg at 25°C
• Boiling Point: 471.7°C at 760 mmHg
• Flash Point: 172°C
• PSA: 82.06000
• Density: 1.166g/cm³
• LogP: 2.39600

Purity/Quality:

99%min ^*data from raw suppliers

3-Methyl-5-oxo-5-(3,4,5-trimethoxyphenyl)valericacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-METHYL-5-OXO-5-(3,4,5-TRIMETHOXYPHENYL)VALERIC ACID

There total 2 articles about 3-METHYL-5-OXO-5-(3,4,5-TRIMETHOXYPHENYL)VALERIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-2-(3,4,5-trimethoxy-benzoyl)-glutaric acid diethyl ester (102601-15-0) → 3-methyl-5-oxo-5-(3,4,5-trimethoxy-phenyl)-valeric acid (101499-91-6)

Guidance literature:

With sulfuric acid;

Reference yield:

ethyl trimethoxybenzoyl acetate (3044-56-2) → 3-methyl-5-oxo-5-(3,4,5-trimethoxy-phenyl)-valeric acid (101499-91-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium ethylate

2: aqueous H₂SO₄

With sulfuric acid; sodium ethanolate;

upstream raw materials:

3-methyl-2-(3,4,5-trimethoxy-benzoyl)-glutaric acid diethyl ester

ethyl trimethoxybenzoyl acetate