o-(3-Methylbenzyl)hydroxylamine

Base Information

Chemical Name:o-(3-Methylbenzyl)hydroxylamine
CAS No.:5555-50-0
Molecular Formula:C8H11NO
Molecular Weight:137.181
Hs Code.:
ChEMBL ID:CHEMBL3765983
DSSTox Substance ID:DTXSID001280289

Synonyms:o-(3-methylbenzyl)hydroxylamine;5555-50-0;O-[(3-methylphenyl)methyl]hydroxylamine;SCHEMBL402229;CHEMBL3765983;DTXSID001280289;MFCD11594364;AKOS006318895;SY281673;CS-0080701;EN300-1246737

Suppliers and Price of o-(3-Methylbenzyl)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of o-(3-Methylbenzyl)hydroxylamine

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:137.084063974
Heavy Atom Count:10
Complexity:95.3

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)CON

Technology Process of o-(3-Methylbenzyl)hydroxylamine

There total 2 articles about o-(3-Methylbenzyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 587-03-1
3-methylbenzyl alcohol

: 5555-50-0
O-[(3-methylphenyl)-methyl]-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: PPh₃; DEAD / tetrahydrofuran / 0 - 50 °C

2: 80 percent / N₂H₄*H₂O / ethanol / 78 °C

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; 1: Mitsunobu reaction;
DOI:10.1016/S0960-894X(03)00713-3