Pentaborane(9), 2-bromo-

Base Information

Chemical Name:Pentaborane(9), 2-bromo-
CAS No.:23753-64-2
Molecular Formula:B₅BrH₈
Molecular Weight:142.023
Hs Code.:

Synonyms:

Suppliers and Price of Pentaborane(9), 2-bromo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pentaborane(9), 2-bromo-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pentaborane(9), 2-bromo-

There total 5 articles about Pentaborane(9), 2-bromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23753-67-5
1-bromopentaborane⁽⁹⁾

: 19624-22-7
pentaborane⁽⁹⁾

: 19495-55-7
1-CH₃B₅H₈

: 121-43-7,63156-11-6
Trimethyl borate

: 23753-64-2
2-bromo-pentaborane⁽⁹⁾

Guidance literature:: With (CH₃)2O; In Dimethyl ether; byproducts: H2, CH3Br; at 24°C, 48h;;
DOI:10.1021/ja01094a055

Reference yield:

: 53451-55-1
(CH₃(CH₂)3)4N⁽¹⁺⁾*B₃H₈^(1-)=(CH₃(CH₂)3)4NB₃H₈

: 10294-33-4
boron tribromide

: 18283-93-7
tetraborane

: 76522-06-0
(CH₃(CH₂)3)4N⁽¹⁺⁾*HBBr₃^(1-)=(CH₃(CH₂)3)4NHBBr₃

: 23753-64-2
2-bromo-pentaborane⁽⁹⁾

: 23753-64-2
BrB₄H₉

: 19287-45-7
diborane

Guidance literature:: With HBr; In dichloromethane; byproducts: H2; HBr condensing onto ammonium borate in CH2Cl2 at -196°C, warmingto -78°C for 1 h, then stirring at room temp.for several minutes, BBr3 and CH2Cl2 condensing at -196°C, stirring at -78°C for 12 h, fractionating; identified by IR and NMR spectra;
DOI:10.1021/ic00135a048

Reference yield:

: 53451-55-1
(CH₃(CH₂)3)4N⁽¹⁺⁾*B₃H₈^(1-)=(CH₃(CH₂)3)4NB₃H₈

: 10294-33-4
boron tribromide

: 18283-93-7
tetraborane

: 76522-06-0
(CH₃(CH₂)3)4N⁽¹⁺⁾*HBBr₃^(1-)=(CH₃(CH₂)3)4NHBBr₃

: 23753-64-2
2-bromo-pentaborane⁽⁹⁾

: 23753-64-2
BrB₄H₉

: 19287-45-7
diborane

Guidance literature:: With HBr; In dichloromethane; byproducts: H2; HBr condensing onto ammonium borate in CH2Cl2 at -196°C, warmingto -78°C for 1 h, then stirring at room temp.for several minutes, BBr3 and CH2Cl2 condensing at -196°C, stirring at -78°C for 12 h, fractionating; identified by IR and NMR spectra;
DOI:10.1021/ic00135a048