(R)-1-(4-(TrifluoroMethoxy)phenyl)ethanaMine hydrochloride

Base Information

• Chemical Name: (R)-1-(4-(TrifluoroMethoxy)phenyl)ethanaMine hydrochloride
• CAS No.: 1208989-29-0
• Molecular Formula: C9H11ClF3NO
• Molecular Weight: 241.641
• Mol file: 1208989-29-0.mol

Synonyms:(R)-1-(4-(TrifluoroMethoxy)phenyl)ethanaMine hydrochloride;(R)-1-(4-(TRIFLUOROMETHOXY)PHENYL)ETHANAMINE HCl

Chemical Property of (R)-1-(4-(TrifluoroMethoxy)phenyl)ethanaMine hydrochloride

Chemical Property:

• PSA: 35.25000
• LogP: 4.10720
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

(R)-1-(4-(Trifluoromethoxy)phenyl)ethanamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R)-1-(4-(TrifluoroMethoxy)phenyl)ethanaMine hydrochloride

There total 3 articles about (R)-1-(4-(TrifluoroMethoxy)phenyl)ethanaMine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H18F3NO2S (1208989-28-9) → (R)-1-(4-(trifluoromethoxy)phenyl)ethanamine hydrochloride (1208989-29-0,1373925-08-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2 - 3h; Inert atmosphere;

Reference yield:

C12H14F3NO2S → (R)-1-(4-(trifluoromethoxy)phenyl)ethanamine hydrochloride (1208989-29-0,1373925-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -40 - -30 °C

1.2: -50 - -45 °C

2.1: hydrogenchloride / 1,4-dioxane; methanol / 2 - 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; methanol;

Reference yield:

p-trifluoromethoxybenzaldehyde (659-28-9) → (R)-1-(4-(trifluoromethoxy)phenyl)ethanamine hydrochloride (1208989-29-0,1373925-08-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: Ti(O-i-Pr)4 / tetrahydrofuran / 20 - 70 °C

2.1: tetrahydrofuran / -40 - -30 °C

2.2: -50 - -45 °C

3.1: hydrogenchloride / 1,4-dioxane; methanol / 2 - 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; Ti(O-i-Pr)4; In tetrahydrofuran; 1,4-dioxane; methanol;

upstream raw materials:

C₁₃H₁₈F₃NO₂S

p-trifluoromethoxybenzaldehyde

Downstream raw materials:

C₃₀H₃₃F₃N₆O₄S

C₂₇H₂₉F₃N₆O₄S

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