Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy-

Base Information

Chemical Name:Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy-
CAS No.:128425-94-5
Molecular Formula:C₁₈H₂₃NO₅
Molecular Weight:333.384
Hs Code.:
Mol file:128425-94-5.mol

Synonyms:Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy-

Suppliers and Price of Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy-

Chemical Property:

PSA：68.23000
LogP:2.49800

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy-

There total 3 articles about Spiro[cyclohexane-1,1(5H)-[3H]oxazolo[4,3-a]isoquinolin]-3-one, 6,10b-dihydro-10b-hydroxy-8,9-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 128425-95-6
Methyl 1-Cyclohexylidene-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

: 128425-94-5
1,5,6,10b-Tetrahydro-10b-hydroxy-8,9-dimethoxy-1,1-pentamethylene-3H-oxazolo<4,3-a>isoquinolin-3-one

Guidance literature:: With lead(IV) acetate; acetic acid; for 2.5h;

Reference yield: 80.0%

: 128425-93-4
Phenyl 1-Cyclohexylidene-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-2-carboxylate

: 128425-94-5
1,5,6,10b-Tetrahydro-10b-hydroxy-8,9-dimethoxy-1,1-pentamethylene-3H-oxazolo<4,3-a>isoquinolin-3-one

Guidance literature:: With lead(IV) acetate; acetic acid; for 0.5h;

Reference yield:

: 69743-45-9
1-cyclohexyl-3,4-dihydro-6,7-dimethoxyisoquinoline

: 128425-94-5
1,5,6,10b-Tetrahydro-10b-hydroxy-8,9-dimethoxy-1,1-pentamethylene-3H-oxazolo<4,3-a>isoquinolin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Di-isopropylethylamine / CH₂Cl₂ / 18 h

2: 80 percent / Pb(OAc)4, glac. acetic acid / 2.5 h

With lead(IV) acetate; acetic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;