5-bromo-6-methyl-1H-Indole-3-carboxaldehyde

Base Information

Chemical Name:5-bromo-6-methyl-1H-Indole-3-carboxaldehyde
CAS No.:1368319-66-7
Molecular Formula:C10H8BrNO
Molecular Weight:238.084
Hs Code.:
Mol file:1368319-66-7.mol

Synonyms:5-bromo-6-methyl-1H-Indole-3-carboxaldehyde;5-bromo-6-methyl-1H-indole-3-carbaldehyde

Suppliers and Price of 5-bromo-6-methyl-1H-Indole-3-carboxaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
5-Bromo-6-methyl-1H-indole-3-carbaldehyde 95+%
1g
$ 763.00

Chemenu
5-Bromo-6-methyl-1H-indole-3-carbaldehyde 95%
1g
$ 721.00

Alichem
5-Bromo-6-methyl-1H-indole-3-carbaldehyde
1g
$ 795.76

Total 4 raw suppliers

Chemical Property of 5-bromo-6-methyl-1H-Indole-3-carboxaldehyde

Chemical Property:

PSA：32.86000
LogP:3.05130

Purity/Quality:

98% ^*data from raw suppliers

5-Bromo-6-methyl-1H-indole-3-carbaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-bromo-6-methyl-1H-Indole-3-carboxaldehyde

There total 1 articles about 5-bromo-6-methyl-1H-Indole-3-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1000343-13-4
5-bromo-6-methyl-1H-indole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1368319-66-7
5-bromo-6-methyl-1H-indole-3-carbaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; for 0.0833333h;

5-bromo-6-methyl-1H-indole;

With sodium hydroxide; at 100 ℃; for 0.0166667h; pH=10;

Reference yield: 74.0%

: 1467060-42-9
{1-[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]cyclopropyl}methanol

: 1368319-66-7
5-bromo-6-methyl-1H-indole-3-carbaldehyde

: 1467060-51-0
5-{4-[1-(hydroxymethyl)cyclopropyl]phenyl}-6-methyl-1H-indole-3-carbaldehyde

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In ethanol; water; toluene; at 20 ℃; Inert atmosphere;

Reference yield:

: 1467060-42-9
{1-[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]cyclopropyl}methanol

: 1368319-66-7
5-bromo-6-methyl-1H-indole-3-carbaldehyde

: 1467057-82-4
5-{4-[1-(hydroxymethyl)cyclopropyl]phenyl}-6-methyl-1H-indole-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / water; ethanol; toluene / 20 °C / Inert atmosphere

2: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogen phosphate / water; acetonitrile; tert-butyl alcohol / 18 h / 0 - 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium chlorite; sodium dihydrogen phosphate; 2-methyl-but-2-ene; potassium carbonate; In ethanol; water; toluene; acetonitrile; tert-butyl alcohol;