C-QUINOLIN-3-YL-METHYLAMINE DIHYDROCHLORIDE

Base Information

• Chemical Name: C-QUINOLIN-3-YL-METHYLAMINE DIHYDROCHLORIDE
• CAS No.: 31842-22-5
• Molecular Formula: C₁₀H₁₀N₂*ClH
• Molecular Weight: 194.664
• Hs Code.: 2933499090
• Mol file: 31842-22-5.mol

Synonyms:C-QUINOLIN-3-YL-METHYLAMINE DIHYDROCHLORIDE

Chemical Property of C-QUINOLIN-3-YL-METHYLAMINE DIHYDROCHLORIDE

Chemical Property:

• Melting Point: 225-230 °C (decomp)
• PSA: 38.91000
• LogP: 3.99780
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

Quinolin-3-ylmethanamine dihydrochloride 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C-QUINOLIN-3-YL-METHYLAMINE DIHYDROCHLORIDE

There total 2 articles about C-QUINOLIN-3-YL-METHYLAMINE DIHYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C15H18N2O2 (1072806-70-2) → quinolin-3-ylmethanaminium chloride (1072806-51-9,31842-22-5)

Guidance literature:

C₁₅H₁₈N₂O₂; With trifluoroacetic acid; In dichloromethane; for 1h;

With hydrogenchloride; In 1,4-dioxane; dichloromethane;

Reference yield:

3-cyanoquinoline (34846-64-5) → quinolin-3-ylmethanaminium chloride (1072806-51-9,31842-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate; nickel dichloride / methanol / 1.33 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 1 h

With sodium tetrahydroborate; trifluoroacetic acid; nickel dichloride; In methanol; dichloromethane;

upstream raw materials:

C₁₅H₁₈N₂O₂

3-cyanoquinoline

Refernces