6-broMo-3,3-diMethylindoline

Base Information

Chemical Name:6-broMo-3,3-diMethylindoline
CAS No.:158326-85-3
Molecular Formula:C10H12BrN
Molecular Weight:226.116
Hs Code.:2933990090
Mol file:158326-85-3.mol

Synonyms:6-broMo-3,3-diMethylindoline

Suppliers and Price of 6-broMo-3,3-diMethylindoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Bromo-3,3-dimethylindoline
5mg
$ 60.00

Matrix Scientific
6-Bromo-3,3-dimethylindoline 95%
1g
$ 7030.00

Labseeker
6-bromo-3,3-dimethylindoline 95
10g
$ 2933.00

Crysdot
6-bromo-3,3-dimethylindoline 95+%
1g
$ 1032.00

American Custom Chemicals Corporation
6-BROMO-3,3-DIMETHYLINDOLINE 95.00%
5MG
$ 496.96

Alichem
6-Bromo-3,3-dimethylindoline
5g
$ 2201.62

Alichem
6-Bromo-3,3-dimethylindoline
1g
$ 685.08

Alichem
6-Bromo-3,3-dimethylindoline
250mg
$ 293.62

Total 9 raw suppliers

Chemical Property of 6-broMo-3,3-diMethylindoline

Chemical Property:

Boiling Point:270.2±39.0 °C(Predicted)
PKA:4.37±0.40(Predicted)
PSA：12.03000
Density:1.336±0.06 g/cm3(Predicted)
LogP:3.29020

Purity/Quality:

99%, ^*data from raw suppliers

6-Bromo-3,3-dimethylindoline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-broMo-3,3-diMethylindoline

There total 6 articles about 6-broMo-3,3-diMethylindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

: 158326-84-2
6-Bromo-3,3-dimethyl-2-oxo-indole

: 158326-85-3
6-Bromo-3,3-dimethyl-dihydroindole

Guidance literature:: With sodium hydroxide; In toluene;

Reference yield: 73.0%

: 158326-85-3
6-Bromo-3,3-dimethyl-dihydroindole

Guidance literature:

Reference yield:

: 83-34-1
3-Methylindole

: 158326-85-3
6-Bromo-3,3-dimethyl-dihydroindole

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / N-bromophthalimide / benzene

2: 98 percent / H₂SO₄ / dioxane

3: 1.) NaH / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 2 h

4: 98 percent / 1 N aq. NaOH / ethanol / 1 h / Ambient temperature

5: 73 percent / sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 0.25 h / 85 °C

With sodium hydroxide; N-bromophthalimide; sulfuric acid; sodium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In 1,4-dioxane; ethanol; toluene; benzene;
DOI:10.1021/jm950646f