CarbaMic acid, N-Methyl-N-[(3S,4S)-4-Methyl- 3-piperidinyl]-, 1,1-diMethylethyl ester, rel-

Base Information

• Chemical Name: CarbaMic acid, N-Methyl-N-[(3S,4S)-4-Methyl- 3-piperidinyl]-, 1,1-diMethylethyl ester, rel-
• CAS No.: 1419075-90-3
• Molecular Formula: C₁₂H₂₄N₂O₂
• Molecular Weight: 228.335
• Mol file: 1419075-90-3.mol

Synonyms:CarbaMic acid, N-Methyl-N-[(3S,4S)-4-Methyl- 3-piperidinyl]-, 1,1-diMethylethyl ester, rel-;tert-Butyl Methyl((3S,4S)-4-Methylpiperidin-3-yl)carbaMate;tert-butyl N-methyl-N-[(3S,4S)-4-methylpiperidin-3-yl]carbamate

Chemical Property of CarbaMic acid, N-Methyl-N-[(3S,4S)-4-Methyl- 3-piperidinyl]-, 1,1-diMethylethyl ester, rel-

Chemical Property:

• PSA: 41.57000
• LogP: 2.18010

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butylmethyl((3S,4S)-4-methylpiperidin-3-yl)carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CarbaMic acid, N-Methyl-N-[(3S,4S)-4-Methyl- 3-piperidinyl]-, 1,1-diMethylethyl ester, rel-

There total 13 articles about CarbaMic acid, N-Methyl-N-[(3S,4S)-4-Methyl- 3-piperidinyl]-, 1,1-diMethylethyl ester, rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

tert-butyl N-[(3R,4R)-1-benzyl-4-methylpiperidin-3-yl]-N-methylcarbamate → tert-butyl N-methyl-N-[(3R,4R)-4-methylpiperidin-3-yl]carbamate (1206824-89-6,1419075-90-3)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 10h;

Reference yield: 97.0%

tert-butyl (1-benzyl-4-methylpiperidin-3-yl)methylcarbamate → tert-butyl methyl(4-methylpiperidin-3-yl)carbamate (1206824-89-6,1419075-90-3)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; for 20h;

Reference yield: 97.0%

tert-butyl (1-benzyl-4-methylpiperidin-3-yl)methylcarbamate → tert-butyl methyl(4-methylpiperidin-3-yl)carbamate (1206824-89-6,1419075-90-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; for 20h;

upstream raw materials:

di-tert-butyl dicarbonate

N-(3R,4R)-(1-benzyl-4-methylpiperidin-3-yl)-methylamine

cis-N-benzyl-3-methoxycarbonylamino-4-methylpiperidine

cis-1-benzyl-N,4-dimethylpiperidin-3-amine

Downstream raw materials:

3-[(3R,4R)-3-({2-chloro-7H-pyrrolo[2,3-d]pyrimidin-4-yl}(methyl)amino)-4-methylpiperidin-1-yl]-3-oxopropanenitrile

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