Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]-

Base Information

Chemical Name:Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]-
CAS No.:1115639-90-1
Molecular Formula:C36H22S
Molecular Weight:486.62
Hs Code.:
Mol file:1115639-90-1.mol

Synonyms:Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]-;4-(3-(triphenylen-2-yl)phenyl)dibenzo[b,d]thiophene;4-[3-(2-triphenylenyl)phenyl]-Dibenzothiophene

Suppliers and Price of Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 9 raw suppliers

Chemical Property of Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]-

Chemical Property:

PSA：28.24000
LogP:10.84810

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]-

There total 4 articles about Dibenzothiophene, 4-[3-(2-triphen ylenyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108847-20-7
4-dibenzothiophene boronic acid

: 1395888-84-2
2-(3-iodophenyl)triphenylene

: 1115639-90-1
4-(3-(triphenylen-2-yl)phenyl)dibenzo[b,d]thiophene

Guidance literature:: In toluene; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.dyepig.2013.09.046

Reference yield:

: 19111-87-6
2-bromobenzo[9,10]phenanthrene

: 1115639-90-1
4-(3-(triphenylen-2-yl)phenyl)dibenzo[b,d]thiophene

Guidance literature:: Multi-step reaction with 3 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 24 h / Inert atmosphere; Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene / 48 h / 90 °C / Inert atmosphere

3: toluene / 24 h / 120 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; In 1,4-dioxane; toluene;
DOI:10.1016/j.dyepig.2013.09.046