1-(4-methoxybenzyl)-6,6-dimethyl-6,7-dihydro-1H-indazol-4(5H)-one

Base Information

Chemical Name:1-(4-methoxybenzyl)-6,6-dimethyl-6,7-dihydro-1H-indazol-4(5H)-one
CAS No.:1355248-91-7
Molecular Formula:C₁₇H₂₀N₂O₂
Molecular Weight:284.358
Hs Code.:
Mol file:1355248-91-7.mol

Synonyms:1-(4-methoxybenzyl)-6,6-dimethyl-6,7-dihydro-1H-indazol-4(5H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxybenzyl)-6,6-dimethyl-6,7-dihydro-1H-indazol-4(5H)-one

Chemical Property:

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Technology Process of 1-(4-methoxybenzyl)-6,6-dimethyl-6,7-dihydro-1H-indazol-4(5H)-one

There total 3 articles about 1-(4-methoxybenzyl)-6,6-dimethyl-6,7-dihydro-1H-indazol-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 824-94-2
p-methoxybenzyl chloride

: 912259-11-1,150352-17-3
6,6-dimethyl-1⁽²⁾,5,6,7-tetrahydro-4H-indazole-4-one

: 1355248-91-7
C₁₇H₂₀N₂O₂

: 1355248-92-8
C₁₇H₂₀N₂O₂

Guidance literature:: With potassium carbonate; In acetonitrile; for 6h; Reflux;

Reference yield:

: 126-81-8
dimedone

: 1355248-91-7
C₁₇H₂₀N₂O₂

: 1355248-92-8
C₁₇H₂₀N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1 h / 20 °C

2: hydrazine hydrate; acetic acid / ethanol / 17 h / 0 °C / Reflux

3: potassium carbonate / acetonitrile / 6 h / Reflux

With potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; acetonitrile;

Reference yield:

: 75039-59-7
2-dimethylaminomethylene-5,5-dimethylcyclohexane-1,3-dione

: 1355248-91-7
C₁₇H₂₀N₂O₂

: 1355248-92-8
C₁₇H₂₀N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate; acetic acid / ethanol / 17 h / 0 °C / Reflux

2: potassium carbonate / acetonitrile / 6 h / Reflux

With potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; acetonitrile;