Ethyl N-Cbz-3-piperidineacetate

Base Information

• Chemical Name: Ethyl N-Cbz-3-piperidineacetate
• CAS No.: 953079-96-4
• Molecular Formula: C17H23NO4
• Molecular Weight: 305.36882
• Mol file: 953079-96-4.mol

Synonyms:Ethyl N-Cbz-3-piperidineacetate;benzyl 3-(2-ethoxy-2-oxoethyl)piperidine-1-carboxylate

Chemical Property of Ethyl N-Cbz-3-piperidineacetate

Chemical Property:

• PSA: 55.84000
• LogP: 2.92630

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl N-Cbz-3-piperidineacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl N-Cbz-3-piperidineacetate

There total 2 articles about Ethyl N-Cbz-3-piperidineacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-(piperidin-3-yl)acetate (64995-88-6,81290-45-1) + benzyl chloroformate (501-53-1,94274-21-2) → 3-ethoxycarbonylmethyl-piperidine-1-carboxylic acid benzyl ester (953079-96-4)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

pyridin-3-yl-acetic acid ethyl ester (39931-77-6) → 3-ethoxycarbonylmethyl-piperidine-1-carboxylic acid benzyl ester (953079-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / Rh/Al₂O₃ / ethanol / 16 h / 60 °C / 3102.97 Torr

2: triethylamine / tetrahydrofuran / 2 h / 0 °C

With hydrogen; triethylamine; Rh/Al₂O₃; In tetrahydrofuran; ethanol;

upstream raw materials:

ethyl 2-(piperidin-3-yl)acetate

benzyl chloroformate

pyridin-3-yl-acetic acid ethyl ester

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