(3-BroMophenyl)(2,4,6-triMethylphenyl)iodoniuM triflate

Base Information

• Chemical Name: (3-BroMophenyl)(2,4,6-triMethylphenyl)iodoniuM triflate
• CAS No.: 1203709-76-5
• Molecular Formula: C16H15BrF3IO3S
• Molecular Weight: 551.163
• Mol file: 1203709-76-5.mol

Synonyms:(3-BroMophenyl)(2,4,6-triMethylphenyl)iodoniuM triflate;(3-Bromophenyl)(2,4,6-trimethylphenyl)iodonium trifluoromethanesulfonate;(3-Bromophenyl)mesityliodonium triflate

Chemical Property of (3-BroMophenyl)(2,4,6-triMethylphenyl)iodoniuM triflate

Chemical Property:

• Melting Point: 170 °C
• PSA: 65.58000
• LogP: 2.63490
• Solubility.: soluble in Methanol

Purity/Quality:

95% ^*data from raw suppliers

(3-Bromophenyl)(mesityl)iodonium Trifluoromethanesulfonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 20041340
• Hazard Codes: T
• Statements: 25-36/37/38
• Safety Statements: 26-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-BroMophenyl)(2,4,6-triMethylphenyl)iodoniuM triflate

There total 1 articles about (3-BroMophenyl)(2,4,6-triMethylphenyl)iodoniuM triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

trifluorormethanesulfonic acid (1493-13-6) + 1-Bromo-3-iodobenzene (591-18-4) + 1,3,5-trimethyl-benzene (108-67-8) → 3'-bromo-2,4,6-trimethyl(diphenyliodonium) trifluoromethanesulfonate (1203709-76-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1021/acs.joc.7b01591

Reference yield: 91.0%

3'-bromo-2,4,6-trimethyl(diphenyliodonium) trifluoromethanesulfonate (1203709-76-5) → (3-bromophenyl)(mesityl)iodonium hexafluorophosphate(V)

Guidance literature:

With sodium hexaflorophosphate; In dichloromethane; water; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/jacs.7b05340

Reference yield: 88.0%

3'-bromo-2,4,6-trimethyl(diphenyliodonium) trifluoromethanesulfonate (1203709-76-5) + 1-methoxy-4-(4-phenylbut-1-yn-1-yl)benzene → 3-(3-bromophenyl)-4-(4-methoxyphenyl)-1,2-dihydronaphthalene (1449689-67-1)

Guidance literature:

With 2,6-di-tert-butyl-pyridine; copper(l) chloride; In 1,2-dichloro-ethane; at 50 ℃; for 36h; Inert atmosphere; Sealed tube;

DOI:10.1021/ja405972h

upstream raw materials:

trifluorormethanesulfonic acid

1-Bromo-3-iodobenzene

1,3,5-trimethyl-benzene

Downstream raw materials:

(S)-2-(3-bromophenyl)-1-octanol

(R)-3-(2-(3-bromophenyl)propanoyl)oxazolidin-2-one

(S)-3-(2-(3-bromophenyl)propanoyl)oxazolidin-2-one

2-(3-bromophenyl)-1-methyl-1H-pyrrole

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