2-Azabicyclo[2.2.1]hept-5-en-3-one, 2-acetyl-, (1S,4R)- (9CI)

Base Information

• Chemical Name: 2-Azabicyclo[2.2.1]hept-5-en-3-one, 2-acetyl-, (1S,4R)- (9CI)
• CAS No.: 200002-40-0
• Molecular Formula: C₈H₉NO₂
• Molecular Weight: 151.165
• Mol file: 200002-40-0.mol

Synonyms:2-Azabicyclo[2.2.1]hept-5-en-3-one, 2-acetyl-, (1S,4R)- (9CI)

Chemical Property of 2-Azabicyclo[2.2.1]hept-5-en-3-one, 2-acetyl-, (1S,4R)- (9CI)

Chemical Property:

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Technology Process of 2-Azabicyclo[2.2.1]hept-5-en-3-one, 2-acetyl-, (1S,4R)- (9CI)

There total 6 articles about 2-Azabicyclo[2.2.1]hept-5-en-3-one, 2-acetyl-, (1S,4R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

acetic anhydride (108-24-7) + 2-azabicyclo[2.2.1.]hept-5-en-3-one (49805-30-3) → (+/-)-cis-2-acetyl-2-azabicyclo<2.2.1>hept-5-en-3-one (162307-09-7,200002-40-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 23h; Heating;

DOI:10.1016/S0957-4166(99)00091-9

Reference yield:

cis-2-acetyl-2-aza-bicyclo[2.2.1]hept-5-en-3-one (200002-40-0) → (1R,4S)-2-acetyl-2-azabicyclo<2.2.1>hept-5-en-3-one (189098-29-1,200002-40-0)

Guidance literature:

Savinase; In tetrahydrofuran; phosphate buffer; at 20 ℃; for 48h; pH=7; Enzymatic reaction;

Reference yield:

acetic anhydride (108-24-7) + (-)-2-azabicyclo[2.2.1]hept-5-en-3-one (79200-56-9) → (1R,4S)-2-acetyl-2-azabicyclo<2.2.1>hept-5-en-3-one (189098-29-1,200002-40-0)

Guidance literature:

With dmap; triethylamine; In chloroform; for 4h; Ambient temperature;

DOI:10.1016/S0040-4039(97)00234-7

upstream raw materials:

acetic anhydride

2-azabicyclo[2.2.1.]hept-5-en-3-one

(-)-2-azabicyclo[2.2.1]hept-5-en-3-one

(+/-)-cis-2-acetyl-2-azabicyclo<2.2.1>hept-5-en-3-one

Downstream raw materials:

(1R,4S)-2-acetyl-2-azabicyclo<2.2.1>hept-5-en-3-one

(1R,4S,5R,6S)-2-acetyl-5,6-dihydroxy-2-azabicyclo-[2.2.1]heptan-3-one

(1S,2R,4S,5R)-6-Acetyl-3-oxa-6-aza-tricyclo[3.2.1.0^2,4]octan-7-one

(1R,4S)-2-Acetyl-1-amino-4-(hydroxymethyl)-2-cyclopentene

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