Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)-

Base Information

Chemical Name:Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)-
CAS No.:436865-51-9
Molecular Formula:C9H11NO3
Molecular Weight:0
Hs Code.:
Mol file:436865-51-9.mol

Synonyms:Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)-

Suppliers and Price of Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)-

Chemical Property:

PSA：66.40000
LogP:0.28720

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)-

There total 2 articles about Acetamide, N-(3-hydroxy-3-methyl-6-oxo-1,4-cyclohexadien-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 436865-50-8
N-(3-hydroperoxy-3-methyl-6-oxocyclohexa-1,4-dienyl)acetamide

: 436865-51-9
N-(3-hydroxy-3-methyl-6-oxocyclohexa-1,4-dienyl)acetamide

Guidance literature:: With titanium(IV) isopropylate; dimethylsulfide; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1055/s-2002-20481

Reference yield:

: 6375-17-3
2-acetylamino-p-cresol

: 436865-51-9
N-(3-hydroxy-3-methyl-6-oxocyclohexa-1,4-dienyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / O₂; meso-tetraphenylporphine / acetone; CH₂Cl₂ / 48 h / -25 °C / Irradiation

2: 83 percent / 4 Angstroem molecular sieves; Me₂S; Ti(O-i-Pr)4 / CH₂Cl₂ / 1 h / 20 °C

With titanium(IV) isopropylate; 5,10,15,20-tetrakisphenylporphyrin; dimethylsulfide; 4 A molecular sieve; oxygen; In dichloromethane; acetone;
DOI:10.1055/s-2002-20481