(S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide

Base Information

• Chemical Name: (S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide
• CAS No.: 1068139-38-7
• Molecular Formula: C23H38N2O3S
• Molecular Weight: 422.632
• Hs Code.: 29350090
• Mol file: 1068139-38-7.mol

Synonyms:(S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide;(S)-HuaCat 95%;(S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide, Mixture of branched isoMers on the dodecyl chain;(S)-HuaCat;(S)-N-(p-Dodecylphenylsulfonyl)-2-pyrrolidinecarboxamide;(2S)-N-[(4-Dodecylphenyl)sulfonyl]-2-pyrrolidinecarboxamide

Chemical Property of (S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide

Chemical Property:

• Melting Point: 203-208°C
• PSA: 83.65000
• LogP: 6.50740

Purity/Quality:

98%,99%, ^*data from raw suppliers

(S)-HuaCat 95% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide

There total 2 articles about (S)-N-(4-Dodecylphenylsulfonyl)pyrrolidine-2-carboxaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C31H44N2O5S (1068139-34-3) → (S)-N-( p-dodecylphenylsulfonyl)-2-pyrrolidinecarboxamide (1068139-38-7)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 24h;

Reference yield:

C28H46N2O5S → (S)-N-( p-dodecylphenylsulfonyl)-2-pyrrolidinecarboxamide (1068139-38-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.tetasy.2013.05.028

Reference yield: 85.0%

(S)-N-( p-dodecylphenylsulfonyl)-2-pyrrolidinecarboxamide (1068139-38-7) → C23H40N2O2S (1254106-78-9)

Guidance literature:

(S)-N-( p-dodecylphenylsulfonyl)-2-pyrrolidinecarboxamide; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h;

With water; In tetrahydrofuran;

DOI:10.1021/jo1015008

upstream raw materials:

C₃₁H₄₄N₂O₅S

Downstream raw materials:

C₂₃H₄₀N₂O₂S

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