6-Methyl-1-phenylnaphthalene

Base Information

• Chemical Name: 6-Methyl-1-phenylnaphthalene
• CAS No.: 29304-61-8
• Molecular Formula: C₁₇H₁₄
• Molecular Weight: 218.298
• DSSTox Substance ID: DTXSID00493478
• Wikidata: Q82340190
• Mol file: 29304-61-8.mol

Synonyms:6-Methyl-1-phenylnaphthalene;29304-61-8;DTXSID00493478;FT-0715080

Chemical Property of 6-Methyl-1-phenylnaphthalene

Chemical Property:

• PSA: 0.00000
• LogP: 4.81520
• XLogP3: 5.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 218.109550447
• Heavy Atom Count: 17
• Complexity: 238

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC2=C(C=C1)C(=CC=C2)C3=CC=CC=C3

Technology Process of 6-Methyl-1-phenylnaphthalene

There total 14 articles about 6-Methyl-1-phenylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

rac-(1S,4R,5R,6S)-5-(phenylethynyl)-6-(m-tolyl)bicyclo[2.2.1]hept-2-ene → 6-methyl-1-phenylnaphthalene (29304-61-8)

Guidance literature:

With palladium diacetate; 2-(pyrazol-1-yl)pyridine; In acetic acid; dimethyl sulfoxide; at 80 ℃; for 16h;

DOI:10.1002/adsc.202100763

Reference yield:

(3-methylphenyl)acetaldehyde (72927-80-1) + phenylacetylene (536-74-3) → 1-methyl-8-phenylnaphthalene + 6-methyl-1-phenylnaphthalene (29304-61-8)

Guidance literature:

With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 80 ℃; for 15h; Overall yield = 44 %; Overall yield = 28.8 mg; Schlenk technique;

DOI:10.1007/s11426-013-4843-7

Reference yield:

7-methyl-4-phenyl-1,2-dihydronaphthalene (29304-60-7) → 6-methyl-1-phenylnaphthalene (29304-61-8)

Guidance literature:

With chloranil; In 1,3,5-trimethyl-benzene; for 18h; Heating;

upstream raw materials:

7-methyl-4-phenyl-1,2-dihydronaphthalene

2-Methylnaphthalene

dibenzoyl peroxide

1,2-dihydro-4-(4-methylphenyl)naphthalene