4-N-PENTYLPHENYLMAGNESIUM BROMIDE

Base Information

• Chemical Name: 4-N-PENTYLPHENYLMAGNESIUM BROMIDE
• CAS No.: 124388-30-3
• Molecular Formula: C11H15BrMg
• Molecular Weight: 251.45
• Mol file: 124388-30-3.mol

Synonyms:4-N-PENTYLPHENYLMAGNESIUM BROMIDE

Chemical Property of 4-N-PENTYLPHENYLMAGNESIUM BROMIDE

Chemical Property:

• PSA: 0.00000
• LogP: 4.06510

Purity/Quality:

98%min ^*data from raw suppliers

4-Pentylphenylmagnesiumbromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-N-PENTYLPHENYLMAGNESIUM BROMIDE

There total 4 articles about 4-N-PENTYLPHENYLMAGNESIUM BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-pentylbromobenzene (51554-95-1) → p-pentylphenylmagnesium bromide (124388-30-3)

Guidance literature:

With magnesium; In tetrahydrofuran;

Reference yield:

bromobenzene (108-86-1,52753-63-6) → p-pentylphenylmagnesium bromide (124388-30-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 62 percent / anhydrous aluminium chloride / 2 h / 70 °C

2: 71 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 6 h / 130 - 180 °C

3: magnesium turnings / tetrahydrofuran

With potassium hydroxide; aluminium trichloride; hydrazine hydrate; magnesium; In tetrahydrofuran; diethylene glycol;

Reference yield:

4'-bromovalerophenone (7295-44-5) → p-pentylphenylmagnesium bromide (124388-30-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / hydrazine hydrate, potassium hydroxide / bis-(2-hydroxy-ethyl) ether / 6 h / 130 - 180 °C

2: magnesium turnings / tetrahydrofuran

With potassium hydroxide; hydrazine hydrate; magnesium; In tetrahydrofuran; diethylene glycol;

upstream raw materials:

4-pentylbromobenzene

bromobenzene

4'-bromovalerophenone

n-valeryl chloride

Downstream raw materials:

3-(4-Pentyl-phenyl)-6-(4-propyl-phenyl)-pyridazine

3r-methyl-4t-propyl-1c-(4'-amyl-4-biphenylyl)cyclohexane

C₃₃H₄₉NO₃

(S)-1,1-bis(4-pentylphenyl)-2-(pyrrolidin-2-yl)ethanol