(11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine

Base Information

Chemical Name:(11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine
CAS No.:1021439-60-0
Molecular Formula:C36H38NO2P
Molecular Weight:547.666181
Hs Code.:
Mol file:1021439-60-0.mol

Synonyms:(11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine

Suppliers and Price of (11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
(11bR)-N,N-Bis((S)-1-phenylethyl)-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine 97%99%ee
250mg
$ 95.00

Ambeed
(11bR)-N,N-Bis((S)-1-phenylethyl)-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine 97%99%ee
100mg
$ 55.00

Total 5 raw suppliers

Chemical Property of (11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

(11bR)-N,N-Bis((S)-1-phenylethyl)-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine 97%99%ee ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine

There total 7 articles about (11bR)-8,9,10,11,12,13,14,15-octahydro-N,N-bis[(1S)-1-phenylethyl]-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1,10024-74-5
(1S,1'S)-bis(1-phenylethyl)amine

: (R)-1,1’-H₈-binaphthyl-2,2’-diyl-chlorophosphite

: 1021439-60-0,948309-50-0
C₃₆H₃₈NO₂P

Guidance literature:: (1S,1'S)-bis(1-phenylethyl)amine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -30 ℃; Inert atmosphere;

(R)-1,1’-H₈-binaphthyl-2,2’-diyl-chlorophosphite; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol800395m

Reference yield: 70.0%

: 65355-00-2,65355-14-8,39648-74-3
5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol

: 21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1,10024-74-5
(1S,1'S)-bis(1-phenylethyl)amine

: 1021439-60-0,948309-50-0
C₃₆H₃₈NO₂P

Guidance literature:: (1S,1'S)-bis(1-phenylethyl)amine;

5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol; Further stages.;
DOI:10.1002/anie.200701529

Reference yield:

: 21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1,10024-74-5
(1S,1'S)-bis(1-phenylethyl)amine

: 39648-74-3,65355-00-2,65355-14-8
(S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol

: 1021439-60-0,948309-50-0
C₃₆H₃₈NO₂P

Guidance literature:: (1S,1'S)-bis(1-phenylethyl)amine; With triethylamine; phosphorus trichloride; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;

(S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol; In dichloromethane; for 12h; Inert atmosphere;
DOI:10.1021/ol503119z