2-Methoxy-4-(tributylstannyl)pyridine

Base Information

• Chemical Name: 2-Methoxy-4-(tributylstannyl)pyridine
• CAS No.: 1204580-72-2
• Molecular Formula: C₁₈H₃₃NOSn
• Molecular Weight: 398.176
• Hs Code.: 2933599590
• Mol file: 1204580-72-2.mol

Synonyms:2-Methoxy-4-(tributylstannyl)pyridine;4-(tributylstannyl)-2-Methoxypyridine;(2-Methoxypyridin-4-yl)tributylstannane

Chemical Property of 2-Methoxy-4-(tributylstannyl)pyridine

Chemical Property:

• Boiling Point: 402.5±55.0 °C(Predicted)
• PKA: 4.66±0.10(Predicted)
• PSA: 22.12000
• LogP: 5.14630

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-4-(tributylstannyl)pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methoxy-4-(tributylstannyl)pyridine

There total 1 articles about 2-Methoxy-4-(tributylstannyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

4-bromo-2-methoxypyridine (100367-39-3) + tributyltin chloride (1461-22-9) → 2-methoxy-4-(tributylstannyl)pyridine (1204580-72-2)

Guidance literature:

4-bromo-2-methoxypyridine; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

tributyltin chloride; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.joc.1c02800

Reference yield:

2-methoxy-4-(tributylstannyl)pyridine (1204580-72-2) + 3-bromo-1-methyl-2-oxo-4-(4-(4-(trifluoromethoxy) phenoxy)piperidin-1-yl)-1,2-dihydroquinoline-6-carbonitrile → 7-(2-methoxypyridin-4-yl)-5-methyl-6-oxo-8-(4-(4-(trifluoromethoxy) phenoxy)piperidin-1-yl)-5,6-dihydro-1,5-naphthyridine-2-carbonitrile

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) chloride; lithium chloride; In dimethyl sulfoxide; at 100 ℃; Sealed tube;

upstream raw materials:

4-bromo-2-methoxypyridine

tributyltin chloride

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