Technology Process of 2-[(2E,5E,7E,9R,10R,11E)-10-hydroxy-3,7,9,11-tetramethyl-trideca-2,5,7,11-tetraenyl]-5,6-dimethoxy-3-methyl-1H-pyridin-4-one
There total 100 articles about 2-[(2E,5E,7E,9R,10R,11E)-10-hydroxy-3,7,9,11-tetramethyl-trideca-2,5,7,11-tetraenyl]-5,6-dimethoxy-3-methyl-1H-pyridin-4-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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871316-26-6
2-[(2E,5E,7E,11E)-(9R,10R)-10-(tert-Butyl-dimethyl-silanyloxy)-3,7,9,11-tetramethyl-trideca-2,5,7,11-tetraenyl]-5,6-dimethoxy-3-methyl-pyridin-4-ol
- Guidance literature:
-
With
4 A molecular sieve; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 50 ℃;
for 18h;
DOI:10.1021/ja055041f
DOI:10.1021/ja0632862
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 50 ℃;
for 15h;
Molecular sieve;
Inert atmosphere;
DOI:10.1021/jacs.8b08974
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 50 ℃;
for 12h;
Molecular sieve;
Inert atmosphere;
DOI:10.1016/j.tetasy.2009.07.044