1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea

Base Information

Chemical Name:1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea
CAS No.:69225-97-4
Molecular Formula:C7H9Cl3N2O4
Molecular Weight:291.5164
Hs Code.:
DSSTox Substance ID:DTXSID70988922
Nikkaji Number:J96.669J
Mol file:69225-97-4.mol

Synonyms:BRN 1813284;1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea;69225-97-4;Urea, 1-(1-acetoxy-2,2,2-trichloroethyl)-3-acetyl-;C7H9Cl3N2O4;C7-H9-Cl3-N2-O4;DTXSID70988922;LS-158735;Acetamide, N-[[[1-(acetyloxy)-2,2,2-trichloroethyl]amino]carbonyl]-;N-[{[1-(Acetyloxy)-2,2,2-trichloroethyl]imino}(hydroxy)methyl]ethanimidic acid

Suppliers and Price of 1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：91.48000
Density:1.502g/cm³
LogP:2.13620
XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:289.962790
Heavy Atom Count:16
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC(=O)NC(C(Cl)(Cl)Cl)OC(=O)C

Technology Process of 1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea

There total 1 articles about 1-(1-Acetoxy-2,2,2-trichloroethyl)-3-acetylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.7%

: 2000-40-0
(2,2,2-trichloro-1-hydroxyethyl)urea

: 108-24-7
acetic anhydride

: 69225-97-4
N-[(1-acetoxy-2,2,2-trichloro)ethyl]-N'-acetylurea

Guidance literature:: With sulfuric acid;
DOI:10.1016/j.tet.2009.11.099

Reference yield: 88.1%

: 69225-97-4
N-[(1-acetoxy-2,2,2-trichloro)ethyl]-N'-acetylurea

: 31378-03-7
1-phenyl-2-tosylethanone

: (2RS,3SR)-N-acetyl-N'-[(1,1,1-trichloro-4-oxo-4-phenyl-3-tosyl)but-2-yl]urea

Guidance literature:: 1-phenyl-2-tosylethanone; With sodium hydride; In acetonitrile; mineral oil; at 20 ℃; for 0.15h; Cooling with ice;

N-[(1-acetoxy-2,2,2-trichloro)ethyl]-N'-acetylurea; In acetonitrile; mineral oil; at 20 ℃; for 7.73333h; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tet.2010.06.058

Reference yield:

: 5366-49-4
4-toluenesulfonylacetone

: 69225-97-4
N-[(1-acetoxy-2,2,2-trichloro)ethyl]-N'-acetylurea

: (2RS,3RS)-N-acetyl-N'-[(1,1,1-trichloro-4-oxo-3-tosyl)pent-2-yl]urea

: (2RS,3SR)-N-acetyl-N'-[(1,1,1-trichloro-4-oxo-3-tosyl)pent-2-yl]urea

Guidance literature:: 4-toluenesulfonylacetone; With sodium hydride; In acetonitrile; mineral oil; at 20 ℃; for 0.15h; Cooling with ice;

N-[(1-acetoxy-2,2,2-trichloro)ethyl]-N'-acetylurea; In acetonitrile; mineral oil; at 20 ℃; for 8.7h; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tet.2010.06.058