Dithiocarbonic acid S,S-bis(p-chlorophenyl) ester

Base Information

• Chemical Name: Dithiocarbonic acid S,S-bis(p-chlorophenyl) ester
• CAS No.: 24455-27-4
• Molecular Formula: C₁₃H₈Cl₂OS₂
• Molecular Weight: 315.24
• Mol file: 24455-27-4.mol

Synonyms:Dithiocarbonic acid S,S-bis(p-chlorophenyl) ester

Chemical Property of Dithiocarbonic acid S,S-bis(p-chlorophenyl) ester

Chemical Property:

• Boiling Point: 419.3±45.0 °C(Predicted)
• Density: 1.47±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dithiocarbonic acid S,S-bis(p-chlorophenyl) ester

There total 3 articles about Dithiocarbonic acid S,S-bis(p-chlorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

chloro-thioformic acid (4-chloro-phenyl)ester (13606-10-5) + p-Chlorothiophenol (106-54-7) → S,S'-bis-p-chlorophenyl dithiocarbonate (24455-27-4)

Guidance literature:

With potassium hydroxide; In water; acetone; at 25 - 30 ℃; for 24h;

Reference yield: 79.0%

chloro-thioformic acid (4-chloro-phenyl)ester (13606-10-5) → S,S'-bis-p-chlorophenyl dithiocarbonate (24455-27-4)

Guidance literature:

With potassium cyanocarbonimidodithioate; In water; acetone; 0-10 deg C, 5 h. then 25-30 deg C, 1 h.;

Reference yield:

1,2-dithio-oxalic acid S,S'-bis-(4-chloro-phenyl ester) (24455-25-2) → S,S'-bis-p-chlorophenyl dithiocarbonate (24455-27-4)

Guidance literature:

Irradiation;

upstream raw materials:

chloro-thioformic acid (4-chloro-phenyl)ester

p-Chlorothiophenol

1,2-dithio-oxalic acid S,S'-bis-(4-chloro-phenyl ester)

Refernces