5-bromo-2-methoxynicotinamide

Base Information

• Chemical Name: 5-bromo-2-methoxynicotinamide
• CAS No.: 1245646-66-5
• Molecular Formula: C7H7BrN2O2
• Molecular Weight: 231.04668
• Hs Code.: 2933399090
• Mol file: 1245646-66-5.mol

Synonyms:5-bromo-2-methoxynicotinamide

Chemical Property of 5-bromo-2-methoxynicotinamide

Chemical Property:

• Boiling Point: 293.8±40.0 °C(Predicted)
• PKA: 13.80±0.50(Predicted)
• PSA: 65.21000
• Density: 1.632±0.06 g/cm3(Predicted)
• LogP: 1.65190
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

5-Bromo-2-methoxynicotinamide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-bromo-2-methoxynicotinamide

There total 2 articles about 5-bromo-2-methoxynicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.4%

5-bromo-2-methoxy-nicotinic acid (54916-66-4) → 5-bromo-2-methoxynicotinamide (1245646-66-5)

Guidance literature:

5-bromo-2-methoxy-nicotinic acid; With oxalyl dichloride; In dichloromethane; at 0 - 20 ℃; for 4h;

With ammonium hydroxide; In dichloromethane; at 0 ℃; for 0.166667h;

Reference yield:

2-methoxynicotinic acid (16498-81-0) → 5-bromo-2-methoxynicotinamide (1245646-66-5)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / water / 20 °C

2: oxalyl dichloride / dichloromethane / 4 h / 0 - 20 °C

With oxalyl dichloride; bromine; In dichloromethane; water;

upstream raw materials:

2-methoxynicotinic acid

5-bromo-2-methoxy-nicotinic acid

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