6-Azatricyclo[3.2.1.02,4]octan-7-one,(1R,2S,4R,5S)-rel-(9CI)

Base Information

Chemical Name:6-Azatricyclo[3.2.1.02,4]octan-7-one,(1R,2S,4R,5S)-rel-(9CI)
CAS No.:452324-46-8
Molecular Formula:C7H9NO
Molecular Weight:123.15246
Hs Code.:
Mol file:452324-46-8.mol

Synonyms:6-Azatricyclo[3.2.1.02,4]octan-7-one,(1R,2S,4R,5S)-rel-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Azatricyclo[3.2.1.02,4]octan-7-one,(1R,2S,4R,5S)-rel-(9CI)

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Technology Process of 6-Azatricyclo[3.2.1.02,4]octan-7-one,(1R,2S,4R,5S)-rel-(9CI)

There total 2 articles about 6-Azatricyclo[3.2.1.02,4]octan-7-one,(1R,2S,4R,5S)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 79200-56-9
(-)-2-azabicyclo[2.2.1]hept-5-en-3-one

: 452324-46-8,452324-62-8
(-)-exo-7-azatricyclo[3.2.1.0^2.4]octan-6-one

Guidance literature:: palladium diacetate; In diethyl ether; at 20 ℃; for 24h;
DOI:10.1016/S0968-0896(02)00063-9

Reference yield: 52.15%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 49805-30-3
2-azabicyclo[2.2.1.]hept-5-en-3-one

: 452324-46-8,452324-62-8
(+/-)-cis-exo-7-azatricyclo[3.2.1.0^2.4]octan-6-one

Guidance literature:: palladium diacetate; In diethyl ether; at 20 ℃; for 24h;
DOI:10.1016/S0968-0896(02)00063-9

Reference yield:

: 452324-46-8,452324-62-8
(+/-)-cis-exo-7-azatricyclo[3.2.1.0^2.4]octan-6-one

: 452324-48-0,512790-53-3
(+/-)-cis-exo-2-amino-4-hydroxymethyl-bicyclo[3.1.0]hexane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1.5 h / 128 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1016/S0968-0896(02)00063-9