3-chloro-1-PyrrolidineethanaMine

Base Information

Chemical Name:3-chloro-1-PyrrolidineethanaMine
CAS No.:857637-45-7
Molecular Formula:C₆H₁₃ClN₂
Molecular Weight:148.636
Hs Code.:

Synonyms:3-chloro-1-PyrrolidineethanaMine

Suppliers and Price of 3-chloro-1-PyrrolidineethanaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
3-chloro-1-Pyrrolidineethanamine 97.00%
25G
$ 20100.00

AccelPharmtech
3-chloro-1-Pyrrolidineethanamine 97.00%
5G
$ 10700.00

AccelPharmtech
3-chloro-1-Pyrrolidineethanamine 97.00%
1G
$ 6120.00

Total 0 raw suppliers

Chemical Property of 3-chloro-1-PyrrolidineethanaMine

Chemical Property:

PSA：29.26000
LogP:0.89640

Purity/Quality:: 3-chloro-1-Pyrrolidineethanamine 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-chloro-1-PyrrolidineethanaMine

There total 5 articles about 3-chloro-1-PyrrolidineethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 857637-44-6
tert-butyl 2-(3-chloropyrrolidin-1-yl)ethylcarbamate

: 857637-45-7
2-(3-chloropyrrolidin-1yl)ethanamine

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 1h;
DOI:10.1021/jm0608154

Reference yield: 30.0%

: 857637-45-7
2-(3-chloropyrrolidin-1yl)ethanamine

Guidance literature:

Reference yield:

: 857637-07-1,540787-75-5
1-(2-aminoethyl)-pyrrolidin-3-ol

: 857637-45-7
2-(3-chloropyrrolidin-1yl)ethanamine

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / Et₃N / methanol / 16 h

2: Et₃N / CH₂Cl₂

3: 705 mg / tetra-n-butylammonium chloride / dimethylformamide / 0.5 h / 100 °C

4: 30 percent / HCl / ethyl acetate / 1 h

With hydrogenchloride; tetrabutyl-ammonium chloride; triethylamine; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm0608154