13-(4-CHLORO-PHENYL)-3,3-DIMETHYL-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

Base Information

• Chemical Name: 13-(4-CHLORO-PHENYL)-3,3-DIMETHYL-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE
• CAS No.: 1017238-94-6
• Molecular Formula: C23H19ClN2O3
• Molecular Weight: 406.868
• Mol file: 1017238-94-6.mol

Synonyms:13-(4-CHLORO-PHENYL)-3,3-DIMETHYL-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE;13-(4-Chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydroindazolo[1,2-b]phthalazine-1,6,11-tri

Chemical Property of 13-(4-CHLORO-PHENYL)-3,3-DIMETHYL-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

Chemical Property:

• PSA: 61.07000
• LogP: 4.01980

Purity/Quality:

98%Min ^*data from raw suppliers

13-(4-Chlorophenyl)-3,3-dimethyl-2,3,4,13-tetrahydroindazolo[1,2-b]phthalazine-1,6,11-trione 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 13-(4-CHLORO-PHENYL)-3,3-DIMETHYL-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

There total 12 articles about 13-(4-CHLORO-PHENYL)-3,3-DIMETHYL-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,3-dihydrophthalazine-1,4-dione (1445-69-8) + 4-chlorobenzaldehyde (104-88-1) + dimedone (126-81-8) → 3,3-dimethyl-13-(4-chlorophenyl)-3,4-dihydro-2H-indazolo[1,2-b]phthalazine-1,6,11(13H)-trione (1017238-94-6)

Guidance literature:

With nano-γ-aluminasulforic acid; at 110 ℃; for 0.2h;

DOI:10.1016/j.molstruc.2012.11.014

Reference yield: 97.0%

phthalic anhydride (85-44-9) + 4-chlorobenzaldehyde (104-88-1) + dimedone (126-81-8) → 3,3-dimethyl-13-(4-chlorophenyl)-3,4-dihydro-2H-indazolo[1,2-b]phthalazine-1,6,11(13H)-trione (1017238-94-6)

Guidance literature:

With hydrazine hydrate; In neat (no solvent); at 80 ℃; for 0.333333h; Reagent/catalyst;

DOI:10.1039/c6ra06376d

Reference yield: 96.0%

phthalhydrazide + 4-chlorobenzaldehyde (104-88-1) + dimedone (126-81-8) → 3,3-dimethyl-13-(4-chlorophenyl)-3,4-dihydro-2H-indazolo[1,2-b]phthalazine-1,6,11(13H)-trione (1017238-94-6)

Guidance literature:

With O-sulfonated poly(vinylpyrrolidonium)hydrogen sulfate; In neat (no solvent); at 80 ℃; for 0.133333h; Green chemistry;

DOI:10.1039/c6ra08486a

upstream raw materials:

2,3-dihydrophthalazine-1,4-dione

4-chlorobenzaldehyde

dimedone

phthalic anhydride

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