Methyl 6-methoxy-3-nitropicolinate

Base Information

• Chemical Name: Methyl 6-methoxy-3-nitropicolinate
• CAS No.: 1427195-24-1
• Molecular Formula: C₈H₈N₂O₅
• Molecular Weight: 212.162
• Mol file: 1427195-24-1.mol

Synonyms:Methyl 6-methoxy-3-nitropicolinate;6-Methoxy-3-nitro-pyridine-2-carboxylic acid methyl ester

Chemical Property of Methyl 6-methoxy-3-nitropicolinate

Chemical Property:

• PSA: 94.24000
• LogP: 1.30820
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl6-methoxy-3-nitropicolinate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 6-methoxy-3-nitropicolinate

There total 3 articles about Methyl 6-methoxy-3-nitropicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

methyl 6-methoxy-3-nitropicolinimidate → methyl 6-methoxy-3-nitropicolinate (1427195-24-1)

Guidance literature:

With hydrogenchloride; water; In methanol; at 20 ℃; for 6h;

Reference yield:

2,6-dicholoro-3-nitropyridine (16013-85-7,136901-10-5) → methyl 6-methoxy-3-nitropicolinate (1427195-24-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1-methyl-pyrrolidin-2-one / 3 h / 180 °C

2.1: sodium hydroxide / 0.5 h / 20 °C

2.2: 3 h / 20 °C

3.1: water; hydrogenchloride / methanol / 6 h / 20 °C

With 1-methyl-pyrrolidin-2-one; hydrogenchloride; water; sodium hydroxide; In methanol;

Reference yield:

6-chloro-3-nitropicolinonitrile (93683-65-9) → methyl 6-methoxy-3-nitropicolinate (1427195-24-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / 0.5 h / 20 °C

1.2: 3 h / 20 °C

2.1: water; hydrogenchloride / methanol / 6 h / 20 °C

With hydrogenchloride; water; sodium hydroxide; In methanol;

upstream raw materials:

2,6-dicholoro-3-nitropyridine

6-chloro-3-nitropicolinonitrile

Downstream raw materials:

methyl 3-amino-6-methoxy picolinate

3-amino-6-methoxypyridylaldehyde

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