BENZYL-(1-METHYL-1H-PYRROL-2-YLMETHYL)-AMINE

Base Information

• Chemical Name: BENZYL-(1-METHYL-1H-PYRROL-2-YLMETHYL)-AMINE
• CAS No.: 73325-58-3
• Molecular Formula: C13H16N2
• Molecular Weight: 200.28
• Hs Code.: 2933990090
• Mol file: 73325-58-3.mol

Synonyms:BENZYL-(1-METHYL-1H-PYRROL-2-YLMETHYL)-AMINE;N-BENZYL-N-[(1-METHYL-1H-PYRROL-2-YL)METHYL]AMINE;N-BENZYL-1-(1-METHYL-1H-PYRROL-2-YL)METHANAMINE;TIMTEC-BB SBB010992

Chemical Property of BENZYL-(1-METHYL-1H-PYRROL-2-YLMETHYL)-AMINE

Chemical Property:

• PSA: 16.96000
• LogP: 2.70580

Purity/Quality:

99% ^*data from raw suppliers

Benzyl-(1-methyl-1H-pyrrol-2-ylmethyl)-amine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL-(1-METHYL-1H-PYRROL-2-YLMETHYL)-AMINE

There total 6 articles about BENZYL-(1-METHYL-1H-PYRROL-2-YLMETHYL)-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-2-(N-benzyl formimidoyl)pyrrole (69819-52-9) → Benzyl-(1-methyl-1H-pyrrol-2-ylmethyl)-amine (73325-58-3)

Guidance literature:

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; methanol; at 0 - 20 ℃;

DOI:10.1021/jm060882y

Reference yield:

1-methylpyrrole-2-carboxylic acid benzylamide (504434-04-2) → Benzyl-(1-methyl-1H-pyrrol-2-ylmethyl)-amine (73325-58-3)

Guidance literature:

With lithium aluminium tetrahydride; In 1,4-dioxane; for 2h; Heating;

DOI:10.1021/jm00021a009

Reference yield:

N-methylpyrrole aldehyde (1192-58-1) → Benzyl-(1-methyl-1H-pyrrol-2-ylmethyl)-amine (73325-58-3)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / tetrahydrofuran; methanol / 0.5 h / 0 °C

2: sodium cyanoborohydride; HCl / tetrahydrofuran; methanol / 0 - 20 °C

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; methanol;

DOI:10.1021/jm060882y

upstream raw materials:

1-methylpyrrole-2-carboxylic acid benzylamide

1-methyl-2-(N-benzyl formimidoyl)pyrrole

N-methylpyrrole aldehyde

benzylamine

Downstream raw materials:

N-Benzyl-N-(1-methyl-1H-pyrrol-2-ylmethyl)-benzamide

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