1-(3-HYDROXY-6-METHOXY-2-METHYLTETRAHYDRO-2H-PYRAN-4-YL)GUANIDINE

Base Information

• Chemical Name: 1-(3-HYDROXY-6-METHOXY-2-METHYLTETRAHYDRO-2H-PYRAN-4-YL)GUANIDINE
• CAS No.: 442901-00-0
• Molecular Formula: C₈H₁₇N₃O₃
• Molecular Weight: 203.241
• Mol file: 442901-00-0.mol

Synonyms:1-(3-HYDROXY-6-METHOXY-2-METHYLTETRAHYDRO-2H-PYRAN-4-YL)GUANIDINE

Chemical Property of 1-(3-HYDROXY-6-METHOXY-2-METHYLTETRAHYDRO-2H-PYRAN-4-YL)GUANIDINE

Chemical Property:

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Technology Process of 1-(3-HYDROXY-6-METHOXY-2-METHYLTETRAHYDRO-2H-PYRAN-4-YL)GUANIDINE

There total 2 articles about 1-(3-HYDROXY-6-METHOXY-2-METHYLTETRAHYDRO-2H-PYRAN-4-YL)GUANIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

polystyrene-bound 3,5-dimethyl-1H-pyrazole-1-carboxamidine hydrochloride, <= 1.8 mmol active pyrazole-1-carboxamidine groups per gram resin + methyl-3-amino-2,3,6-trideoxy-α-L-lyxo-hexopyranoside (77398-20-0) → N-(1-O-methyl-2,3,6-trideoxy-β-L-lyxo-pyranoside-3-yl)guanidine (442901-00-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 60 ℃; for 24h;

DOI:10.1055/s-2006-926284

Reference yield: 94.0%

methyl-3-amino-2,3,6-trideoxy-α-L-lyxo-hexopyranoside (77398-20-0) → N-(1-O-methyl-2,3,6-trideoxy-β-L-lyxo-pyranoside-3-yl)guanidine (442901-00-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 60 ℃; for 24h;

DOI:10.1016/S0040-4039(01)02403-0

upstream raw materials:

methyl-3-amino-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

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