3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one

Base Information

• Chemical Name: 3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one
• CAS No.: 97389-25-8
• Molecular Formula: C₉H₉NO₃
• Molecular Weight: 179.175
• Hs Code.: 2934999090
• Mol file: 97389-25-8.mol

Synonyms:3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one;2-oxazolidinone, 3-(4-hydroxyphenyl)-;3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one(SALTDATA: FREE);3-(4-hydroxyphenyl)-2-oxazolidinone;3-(4-hydroxyphenyl)oxazolidin-2-one

Chemical Property of 3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one

Chemical Property:

• Vapor Pressure: 2.96E-05mmHg at 25°C
• Boiling Point: 346°C at 760 mmHg
• Flash Point: 163.1°C
• PSA: 49.77000
• Density: 1.378g/cm³
• LogP: 1.41380

Purity/Quality:

97% ^*data from raw suppliers

3-(4-Hydroxyphenyl)-1,3-oxazolidin-2-one ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one

There total 2 articles about 3-(4-hydroxyphenyl)-1,3-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-benzyloxyaniline hydrochloride (51388-20-6) → N-(4-hydroxyphenyl)-1,3-oxazolidin-2-one (97389-25-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / KOH / ethanol / 6 h / Heating

2: 1) HBr / 1) 4 h, reflux, 2) ethyl acetate, RT, overnight

With potassium hydroxide; hydrogen bromide; In ethanol;

Reference yield:

N-(2-hydroxyethyl)-4-benzyloxyaniline (97389-19-0) → N-(4-hydroxyphenyl)-1,3-oxazolidin-2-one (97389-25-8)

Guidance literature:

With hydrogen bromide; Yield given. Multistep reaction; 1) 4 h, reflux, 2) ethyl acetate, RT, overnight;

Reference yield: 62.0%

3,4-dihydro-2H-pyran (110-87-2) + N-(4-hydroxyphenyl)-1,3-oxazolidin-2-one (97389-25-8) → N-(4-tetrahydropyranyloxyphenyl)-1,3-oxazolidin-2-one (97389-26-9)

Guidance literature:

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; Ambient temperature;

upstream raw materials:

N-(2-hydroxyethyl)-4-benzyloxyaniline

4-benzyloxyaniline hydrochloride

Downstream raw materials:

N-(4-tetrahydropyranyloxyphenyl)-1,3-oxazolidin-2-one

N-(2-hydroxyethyl)-O-(tetrahydropyranyl)-p-aminophenol

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