Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate

Base Information

Chemical Name:Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate
CAS No.:254444-59-2
Molecular Formula:C19H26O6S
Molecular Weight:382.478
Hs Code.:

Synonyms:Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate

Suppliers and Price of Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate

There total 1 articles about Ethyl 6-deoxy-2-O-(phenylmethyl)-1-thio-beta-L-galactopyranoside diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 138343-56-3
ethyl 2-O-benzyl-1-thio-β-L-fucopyranoside

: 254444-59-2
ethyl 3,4-di-O-acetyl-2-O-benzyl-1-thio-β-L-fucopyranoside

Guidance literature:: In pyridine; at 20 ℃; for 16h;
DOI:10.1002/1099-0690(200101)2001:1<193::aid-ejoc193>3.0.co;2-s

Reference yield: 86.0%

: 869002-18-6
p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-4-O-(3,4,6-tri-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 254444-59-2
ethyl 3,4-di-O-acetyl-2-O-benzyl-1-thio-β-L-fucopyranoside

: C₉₁H₉₈Cl₃NO₂₆

Guidance literature:: With N-iodo-succinimide; 3 A molecular sieve; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1002/chem.200500412

Reference yield: 83.0%

: 169151-52-4
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: 254444-59-2
ethyl 3,4-di-O-acetyl-2-O-benzyl-1-thio-β-L-fucopyranoside

: 2-azidoethyl O-(3,4-di-O-acetyl-2-O-benzyl-α-L-fucopyranosyl)-(1→3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

Guidance literature:: 2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside; ethyl 3,4-di-O-acetyl-2-O-benzyl-1-thio-β-L-fucopyranoside; In diethyl ether; dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; In diethyl ether; dichloromethane; at -30 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.12.143