[1,2-Bis(dicyclohexylphosphino)ethane]palladiuM(II) chloride,95%

Base Information

• Chemical Name: [1,2-Bis(dicyclohexylphosphino)ethane]palladiuM(II) chloride,95%
• CAS No.: 96165-44-5
• Molecular Formula: C26H48Cl2P2Pd
• Molecular Weight: 599.941
• Mol file: 96165-44-5.mol

Synonyms:[1,2-Bis(dicyclohexylphosphino)ethane]palladiuM(II) chloride,95%;[1,2-Bis(dicyclohexylphosphino)ethane]dichloropalladium;Dichloro[1,2-bis(dicyclohexylphosphino)ethane]palladium;(DCPE)palladium(II) chloride;Dichloro[1,2-bis(dicyclohexylphosphino)ethane]palladium(II)

Chemical Property of [1,2-Bis(dicyclohexylphosphino)ethane]palladiuM(II) chloride,95%

Chemical Property:

• Melting Point: >300°C
• PSA: 27.18000
• LogP: 3.28900
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

[1,2-Bis(dicyclohexylphosphino)ethane]palladium(II) chloride ≥95.0% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22-36/37/38-40-43
• Safety Statements: 26-36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [1,2-Bis(dicyclohexylphosphino)ethane]palladiuM(II) chloride,95%

There total 2 articles about [1,2-Bis(dicyclohexylphosphino)ethane]palladiuM(II) chloride,95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + 1,2-bis-(dicyclohexylphosphino)ethane (23743-26-2) → {1,2-bis(dicyclohexylphosphino)ethane}dichloropalladium(II) (96165-44-5)

Guidance literature:

In toluene; at 25 ℃; for 2h; Inert atmosphere; Glovebox;

DOI:10.1002/anie.202014960

Reference yield: 92.0%

dichloro(1,5-cyclooctadiene)palladium(II) (12107-56-1) + 1,2-bis-(dicyclohexylphosphino)ethane (23743-26-2) → {1,2-bis(dicyclohexylphosphino)ethane}dichloropalladium(II) (96165-44-5)

Guidance literature:

In dichloromethane; (N2); addn. of CH2Cl2 soln. of palladium compd. to CH2Cl2 soln. of phosphine deriv., stirring at room temp. for 4 h; evapn., washing with pentane, drying in vac. for 1 d;

DOI:10.1021/ic901257s

Reference yield: 90.0%

{1,2-bis(dicyclohexylphosphino)ethane}dichloropalladium(II) (96165-44-5) + methyllithium (917-54-4) → (1,2-bis(dicyclohexylphosphino)ethane)dimethylpalladium(II)

Guidance literature:

In diethyl ether; under N2; soln. of MeLi added to soln. of complex at -78°C, brought to room temp.; addn. of H2O, ether and aq. layer filtered off, solid washed (H2O), dried (vac., 1 h, 60°C);

DOI:10.1021/om00042a016

upstream raw materials:

bis(benzonitrile)palladium(II) dichloride

1,2-bis-(dicyclohexylphosphino)ethane

dichloro(1,5-cyclooctadiene)palladium(II)

Downstream raw materials:

{(μ2-1,2-bis(dicyclohexylphosphino)ethane)palladium(0)}2

[(1,2-bis(dicyclohexylphosphino)ethane)Ni(1,2,4,5-benzenetetrathiolate)Pd(1,2-bis(dicyclohexylphosphino)ethane)]

bis(bicarbonato)(1,2-bis(dicyclohexylphosphino)ethane)palladium(II)

[PdH(SiH₂-9-triptycyl)(1,2-bis(dicyclohexylphosphino)ethane)]

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